2-Propanone, 1-(1,3-dithian-2-yl)-

Base Information

Chemical Name:2-Propanone, 1-(1,3-dithian-2-yl)-
CAS No.:18554-39-7
Molecular Formula:C7H12OS2
Molecular Weight:176.304
Hs Code.:
DSSTox Substance ID:DTXSID30448012
Nikkaji Number:J941.879B
Wikidata:Q82266930
Mol file:18554-39-7.mol

Synonyms:2-Propanone, 1-(1,3-dithian-2-yl)-;1-(1,3-dithian-2-yl)propan-2-one;18554-39-7;DTXSID30448012;1-(1,3-Dithiane-2-yl)acetone;1-(1,3-dithian-2-yl) propan-2-one

Suppliers and Price of 2-Propanone, 1-(1,3-dithian-2-yl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 2-Propanone, 1-(1,3-dithian-2-yl)-

Chemical Property:

XLogP3:1.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:176.03295735
Heavy Atom Count:10
Complexity:119

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)CC1SCCCS1

Technology Process of 2-Propanone, 1-(1,3-dithian-2-yl)-

There total 1 articles about 2-Propanone, 1-(1,3-dithian-2-yl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 109-80-8
1.3-propanedithiol

: 625-34-3
3-oxobutyraldehyde

: 18554-39-7
1-(1,3-dithian-2-yl)-2-propanone

Guidance literature:: scandium tris(trifluoromethanesulfonate); In dichloromethane; at 20 ℃; for 1.5h;
DOI:10.1016/S0040-4039(01)02378-4

Reference yield:

: 128461-65-4
3-(p-methoxybenzyloxy)propanal

: 18554-39-7
1-(1,3-dithian-2-yl)-2-propanone

: (R)-1-[1,3]Dithian-2-yl-4-hydroxy-6-(4-methoxy-benzyloxy)-hexan-2-one

: 627536-85-0
(S)-1-[1,3]Dithian-2-yl-4-hydroxy-6-(4-methoxy-benzyloxy)-hexan-2-one

Guidance literature:: 1-(1,3-dithian-2-yl)-2-propanone; With triethylamine; (-)-diisopinocamphenylborane chloride; In dichloromethane; at -78 - 20 ℃;

3-(p-methoxybenzyloxy)propanal; In dichloromethane;
DOI:10.1016/j.tetlet.2003.08.083

Reference yield:

: 18554-39-7
1-(1,3-dithian-2-yl)-2-propanone

: 627537-26-2
(2S,4S)-1-[1,3]Dithian-2-yl-6-(4-methoxy-benzyloxy)-hexane-2,4-diol

Guidance literature:: Multi-step reaction with 2 steps

1.1: (-)-diisopinocamphenylboron chloride; Et₃N / CH₂Cl₂ / -78 - 20 °C

1.2: CH₂Cl₂

2.1: 85 percent / DIBALH / tetrahydrofuran / -78 - -20 °C

With diisobutylaluminium hydride; triethylamine; (-)-diisopinocamphenylborane chloride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2003.08.083