Tricholeine

Base Information

Chemical Name:Tricholeine
CAS No.:62510-52-5
Molecular Formula:
Molecular Weight:
Hs Code.:

Synonyms:

Suppliers and Price of Tricholeine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Tricholeine

Chemical Property:

Purity/Quality:

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Technology Process of Tricholeine

There total 9 articles about Tricholeine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 31642-67-8
non-8-enoic acid

: 62510-52-5
1-[1-oxo-9-(3,4-methylenedioxyphenyl)-8E-nonenyl]-pyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; triethylamine / N,N-dimethyl-formamide; dichloromethane / 0.5 h / 0 °C

1.2: 20 °C

2.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / cis-1,2-Dichloroethylene / 48 h / Reflux

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; triethylamine; In cis-1,2-Dichloroethylene; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c3ra42060d

Reference yield:

: 931-88-4,931-87-3,25267-51-0
cis-Cyclooctene

: 62510-52-5
1-[1-oxo-9-(3,4-methylenedioxyphenyl)-8E-nonenyl]-pyrrolidine

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) O₃, NaHCO₃, 2.) Et₃N / 1.) CH₂Cl₂, MeOH, 2.) CH₂Cl₂, a) 0 deg C, 15 min, b) RT, 4 h

2: 1.) t-BuOK / 1.) THF, DMSO, -10 deg C, 30 min, 2.) THF, -10 deg C

3: NaOH / methanol

4: I₂ / benzene / Ambient temperature

5: 1.) Et₃N / 1.) CH₂Cl₂, 0 deg C, 15 min, 2.) CH₂Cl₂, 30 min

6: CH₂Cl₂ / 1 h

With sodium hydroxide; potassium tert-butylate; iodine; sodium hydrogencarbonate; ozone; triethylamine; In methanol; dichloromethane; benzene;
DOI:10.1248/cpb.45.685

Reference yield:

: 30511-80-9
(8E)-9-(3',4'-methylenedioxyphenyl)-8-nonenoic acid

: 62510-52-5
1-[1-oxo-9-(3,4-methylenedioxyphenyl)-8E-nonenyl]-pyrrolidine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Et₃N / 1.) CH₂Cl₂, 0 deg C, 15 min, 2.) CH₂Cl₂, 30 min

2: CH₂Cl₂ / 1 h

With triethylamine; In dichloromethane;
DOI:10.1248/cpb.45.685