2-[[[4-(Dimethylamino)phenyl]methylene]amino]benzoic acid

Base Information

Chemical Name:2-[[[4-(Dimethylamino)phenyl]methylene]amino]benzoic acid
CAS No.:39900-95-3
Molecular Formula:C16H16 N2 O2
Molecular Weight:268.315
Hs Code.:
European Community (EC) Number:254-694-7
DSSTox Substance ID:DTXSID801197581
Nikkaji Number:J261.477D
Mol file:39900-95-3.mol

Synonyms:39900-95-3;BRN 2736346;2-[[[4-(DIMETHYLAMINO)PHENYL]METHYLENE]AMINO]BENZOIC ACID;EINECS 254-694-7;AI3-20239;2-((((4-Dimethylamino)phenyl)methylene)amino)benzoic acid;Benzoic acid, 2-((((4-dimethylamino)phenyl)methylene)amino)-;2-(4-(dimethylamino)benzylideneamino)benzoic acid;3-14-00-00948 (Beilstein Handbook Reference);2-(((4-(Dimethylamino)phenyl)methylene)amino)benzoic acid;2-[4-(Dimethylamino)benzylideneamino]benzoic acid;Benzoic acid, 2-(((4-(dimethylamino)phenyl)methylene)amino)-;Benzoic acid, 2-[[[4-(dimethylamino)phenyl]methylene]amino]-;DTXSID801197581;STK672736;AKOS001712723;LS-37190;EU-0017972;Benzoic acid, 2-(4-dimethylaminobenzylidenamino)-;2-(((E)-[4-(Dimethylamino)phenyl]methylidene)amino)benzoic acid #;2-({(E)-[4-(dimethylamino)phenyl]methylidene}amino)benzoic acid

Suppliers and Price of 2-[[[4-(Dimethylamino)phenyl]methylene]amino]benzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2-[[[4-(DIMETHYLAMINO)PHENYL]METHYLENE]AMINO]BENZOIC ACID 95.00%
5MG
$ 495.59

Total 5 raw suppliers

Chemical Property of 2-[[[4-(Dimethylamino)phenyl]methylene]amino]benzoic acid

Chemical Property:

Vapor Pressure:2.38E-10mmHg at 25°C
Boiling Point:488.3°C at 760 mmHg
Flash Point:249.1°C
PSA：52.90000
Density:1.11g/cm³
LogP:3.20140
XLogP3:2.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:268.121177757
Heavy Atom Count:20
Complexity:346

Purity/Quality:

99% ^*data from raw suppliers

2-[[[4-(DIMETHYLAMINO)PHENYL]METHYLENE]AMINO]BENZOIC ACID 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(C)C1=CC=C(C=C1)C=NC2=CC=CC=C2C(=O)O

Technology Process of 2-[[[4-(Dimethylamino)phenyl]methylene]amino]benzoic acid

There total 1 articles about 2-[[[4-(Dimethylamino)phenyl]methylene]amino]benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4
anthranilic acid

: 100-10-7
4-dimethylamino-benzaldehyde

: 39900-95-3
N-(p-N,N-dimethylaminobenzylidene)anthranilic acid

Guidance literature:: In neat(no solvent); at 110 ℃; for 0.0166667h; Microwave irradiation;
DOI:10.1002/jhet.604

Reference yield: 72.0%

: 39900-95-3
N-(p-N,N-dimethylaminobenzylidene)anthranilic acid

: 103-80-0
phenylacetyl chloride

: 2-(2-(4-(dimethylamino)phenyl)-4-oxo-3-phenylazetidin-1-yl)-benzoic acid

Guidance literature:: With triethylamine; In dichloromethane; for 16h;
DOI:10.1002/jhet.604

Reference yield: 72.0%

: copper(II) choride dihydrate

: 39900-95-3
N-(p-N,N-dimethylaminobenzylidene)anthranilic acid

: 119541-83-2
Cu(C₁₆H₁₅N₂O₂)ClH₂O

Guidance literature:: In ethanol; treating of soln. of ligand with CuCl2*2H2O (molar ratio 1:1), refluxing (2-6 h), pptn. on evapg. and cooling; sepn. (filtration), washing (EtOH), drying (vac., over preheated CaCl2); elem. anal.;