2(1H)-Phthalazineacetic acid, 1-oxo-, ethyl ester

Base Information

• Chemical Name: 2(1H)-Phthalazineacetic acid, 1-oxo-, ethyl ester
• CAS No.: 18584-72-0
• Molecular Formula: C12H12N2O3
• Molecular Weight: 232.239

Synonyms:1(2H)-oxophthalazin-2-acetic acid ethyl ester;(1-oxo-1H-phthalazin-2-yl)-acetic acid ethyl ester;

Chemical Property of 2(1H)-Phthalazineacetic acid, 1-oxo-, ethyl ester

Chemical Property:

• PSA: 61.19000
• LogP: 0.95960

Purity/Quality:

97% ^*data from raw suppliers

Ethyl (1-oxophthalazin-2(1H)-yl)acetate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2(1H)-Phthalazineacetic acid, 1-oxo-, ethyl ester

There total 1 articles about 2(1H)-Phthalazineacetic acid, 1-oxo-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 1(2H)-oxophthalazin-2-acetic acid ethyl ester (18584-72-0)

Guidance literature:

2-Carboxybenzaldehyd, Hydrazinessigester;

Reference yield: 80.0%

1(2H)-oxophthalazin-2-acetic acid ethyl ester (18584-72-0) → (3,4-dihydro-4-oxophthalizin-3-yl)acetic acid (90689-39-7)

Guidance literature:

With hydrogenchloride; for 2h; Heating;

DOI:10.1080/10426500390228666

Reference yield: 79.0%

p-toluamidoxime (19227-13-5) + 1(2H)-oxophthalazin-2-acetic acid ethyl ester (18584-72-0) → 2-{[3-(4-methylphenyl)-1,2,4-oxadiazol-5-yl]methyl}phthalazin-1(2H)-one

Guidance literature:

With sodium hydroxide; In dimethyl sulfoxide; at 20 ℃; for 4h;

DOI:10.1016/j.tet.2017.01.007

Downstream raw materials:

(3,4-dihydro-4-oxophthalizin-3-yl)acetic acid

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