Biphenyl-3-carboxamide

Base Information

Chemical Name:Biphenyl-3-carboxamide
CAS No.:188665-76-1
Molecular Formula:C13H11NO
Molecular Weight:197.236
Hs Code.:
DSSTox Substance ID:DTXSID501307298
Nikkaji Number:J816.191G

Synonyms:[1,1'-Biphenyl]-3-carboxamide;188665-76-1;biphenyl-3-carboxamide;SCHEMBL43553;SCHEMBL16803129;DTXSID501307298;AKOS002735591;SR-01000650330;SR-01000650330-1

Suppliers and Price of Biphenyl-3-carboxamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Biphenyl-3-carboxamide

Chemical Property:

XLogP3:2.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:197.084063974
Heavy Atom Count:15
Complexity:221

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2=CC(=CC=C2)C(=O)N

Technology Process of Biphenyl-3-carboxamide

There total 3 articles about Biphenyl-3-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: C₁₅H₁₄N₂O

: 24214-73-1,30929-57-8
cyclohexylhydrazine hydrochloride

: 1465766-55-5
5-([1,1'-biphenyl]-3-yl)-1-cyclohexyl-3-methyl-1H-1,2,4-triazole

: 188665-76-1
[1,1’-biphenyl]-3-carboxamide

Guidance literature:: With acetic acid; In N,N-dimethyl-formamide; at 90 ℃; for 6h;

Reference yield:

: 42498-44-2
3-phenylbenzoyl chloride

: 188665-76-1
[1,1’-biphenyl]-3-carboxamide

Guidance literature:: With ammonia; In water;
DOI:10.3998/ark.5550190.0012.808

Reference yield:

: 716-76-7
3-phenylbenzoic acid

: 1465766-55-5
5-([1,1'-biphenyl]-3-yl)-1-cyclohexyl-3-methyl-1H-1,2,4-triazole

: 188665-76-1
[1,1’-biphenyl]-3-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: HATU; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 18 h / 20 °C / Inert atmosphere

2: acetic acid / N,N-dimethyl-formamide / 6 h / 90 °C

With acetic acid; N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide;