3-Hydroxycholan-24-ohydrazide

Base Information

Chemical Name:3-Hydroxycholan-24-ohydrazide
CAS No.:3664-90-2
Molecular Formula:C24H42N2O2
Molecular Weight:390.6025
Hs Code.:
NSC Number:73109
ChEMBL ID:CHEMBL1981487
Mol file:3664-90-2.mol

Synonyms:3664-90-2;NSC 73109;3-Hydroxycholan-24-ohydrazide;NSC73109;MLS002701910;NSC-73109;CHEMBL1981487;NCI60_041596

Suppliers and Price of 3-Hydroxycholan-24-ohydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 3-Hydroxycholan-24-ohydrazide

Chemical Property:

Vapor Pressure:1.66E-14mmHg at 25°C
Boiling Point:552.5°Cat760mmHg
Flash Point:287.9°C
Density:1.067g/cm³
XLogP3:5.3
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:390.324628587
Heavy Atom Count:28
Complexity:595

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(CCC(=O)NN)C1CCC2C1(CCC3C2CCC4C3(CCC(C4)O)C)C
Isomeric SMILES:C[C@H](CCC(=O)NN)[C@H]1CC[C@@H]2[C@@]1(CC[C@H]3[C@H]2CC[C@H]4[C@@]3(CC[C@H](C4)O)C)C

Technology Process of 3-Hydroxycholan-24-ohydrazide

There total 4 articles about 3-Hydroxycholan-24-ohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1249-75-8,5405-42-5,15074-01-8,15074-02-9,20231-51-0,63814-53-9,106757-10-2,125412-30-8
methyl lithocholate

: 3664-90-2
(3α,5β)-3-hydroxycholan-24-hydrazide

Guidance literature:: With hydrazine hydrate; In methanol; at 20 ℃; for 6h; Inert atmosphere;
DOI:10.1002/cmdc.201200102

Reference yield:

: 434-13-9
Lithocholic acid

: 3664-90-2
(3α,5β)-3-hydroxycholan-24-hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid / 3 h / 20 °C / Inert atmosphere

2: hydrazine hydrate / methanol / 6 h / 20 °C / Inert atmosphere

With sulfuric acid; hydrazine hydrate; In methanol;
DOI:10.1002/cmdc.201200102