1,3,2-Benzodioxaborole, 5-(1,1-dimethylethyl)-

Base Information

Chemical Name:1,3,2-Benzodioxaborole, 5-(1,1-dimethylethyl)-
CAS No.:188707-78-0
Molecular Formula:C10H13BO2
Molecular Weight:176.023
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3,2-Benzodioxaborole, 5-(1,1-dimethylethyl)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 1,3,2-Benzodioxaborole, 5-(1,1-dimethylethyl)-

There total 2 articles about 1,3,2-Benzodioxaborole, 5-(1,1-dimethylethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 229024-39-9
(C₅H₅)2Ti(HBO₂C₆H₃C(CH₃)3)(C₆H₅CCC₆H₅)

: 201230-82-2
carbon monoxide

: dicarbonylbis(η-cyclopentadienyl)titanium(II)

: 188707-78-0
5-tert-butyl-1,3,2-benzodioxaborolane

: 501-65-5
diphenyl acetylene

Guidance literature:: In ⁽²⁾H₈-toluene; High Pressure; react. Cp2Ti(PhCCPh)(HBcat') in toluene-d8 with carbon monoxide (610 Torr) at -20°C followed by warming to 40°C; not isolated, identified by NMR spectroscopy;
DOI:10.1021/om990507m

Reference yield:

: 229024-39-9
(C₅H₅)2Ti(HBO₂C₆H₃C(CH₃)3)(C₆H₅CCC₆H₅)

: 201230-82-2
carbon monoxide

: dicarbonylbis(η-cyclopentadienyl)titanium(II)

: 188707-78-0
5-tert-butyl-1,3,2-benzodioxaborolane

: 229024-50-4
PhCHC(Bcat')Ph

: 501-65-5
diphenyl acetylene

Guidance literature:: In ⁽²⁾H₈-toluene; High Pressure; react. Cp2Ti(PhCCPh)(HBcat') in toluene-d8 with carbon monoxide (200 Torr) at -20°C for 2 h; not isolated, identified by NMR spectroscopy;
DOI:10.1021/om990507m

Reference yield: 95.0%

: 637-69-4,24936-44-5
4-Methoxystyrene

: 188707-78-0
5-tert-butyl-1,3,2-benzodioxaborolane

: 256234-72-7
4-MeOC₆H₄CH₂CH₂BO₂C₆H₃-4-t-Bu

Guidance literature:: Cp₂Ti(HBcat')2; In ⁽²⁾H₈-toluene; react. 5-fold excess 4-tert-butylcatecholborane with p-methoxystyrene in C7D8 at -10°C for 1 h in the presence 10 mol % Cp2Ti(HBcat')2;
DOI:10.1021/om990507m