Pentadecanoic acid, 15-chloro-2,2,3,3,4,4-hexafluoro-6-iodo-, phenylmethyl ester

Base Information

• Chemical Name: Pentadecanoic acid, 15-chloro-2,2,3,3,4,4-hexafluoro-6-iodo-, phenylmethyl ester
• CAS No.: 188711-30-0
• Molecular Formula: C22H28ClF6IO2
• Molecular Weight: 600.811
• Mol file: 188711-30-0.mol

Synonyms:

Chemical Property of Pentadecanoic acid, 15-chloro-2,2,3,3,4,4-hexafluoro-6-iodo-, phenylmethyl ester

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Pentadecanoic acid, 15-chloro-2,2,3,3,4,4-hexafluoro-6-iodo-, phenylmethyl ester

There total 1 articles about Pentadecanoic acid, 15-chloro-2,2,3,3,4,4-hexafluoro-6-iodo-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

11-chloroundec-1-ene (872-17-3) + Benzyl 4-iodo-2,2,3,3,4,4-hexafluorobutanoate (188711-29-7) → 15-Chloro-2,2,3,3,4,4-hexafluoro-6-iodo-pentadecanoic acid benzyl ester (188711-30-0)

Guidance literature:

With 2,2'-azobis(isobutyronitrile); In n-heptane; at 90 ℃; for 4h;

DOI:10.1039/a700085e

Reference yield: 72.0%

15-Chloro-2,2,3,3,4,4-hexafluoro-6-iodo-pentadecanoic acid benzyl ester (188711-30-0) → 15-Chloro-2,2,3,3,4,4-hexafluoro-pentadecanoic acid benzyl ester

Guidance literature:

With acetic acid; zinc; In 2,2,4-trimethylpentane; at 110 ℃; for 2h;

DOI:10.1039/a700085e

Reference yield:

15-Chloro-2,2,3,3,4,4-hexafluoro-6-iodo-pentadecanoic acid benzyl ester (188711-30-0) → 15-(4'-Cyano-biphenyl-4-yloxy)-2,2,3,3,4,4-hexafluoro-pentadecanoic acid benzyl ester

Guidance literature:

Multi-step reaction with 2 steps

1: 72 percent / Zn, AcOH / 2,2,4-trimethyl-pentane / 2 h / 110 °C

2: K₂CO₃ / dimethylformamide / 3 h / 90 °C

With potassium carbonate; acetic acid; zinc; In 2,2,4-trimethylpentane; N,N-dimethyl-formamide;

DOI:10.1039/a700085e

upstream raw materials:

11-chloroundec-1-ene

Benzyl 4-iodo-2,2,3,3,4,4-hexafluorobutanoate