Ethyl (2E)-2-(dimethylhydrazinylidene)propanoate

Base Information

Chemical Name:Ethyl (2E)-2-(dimethylhydrazinylidene)propanoate
CAS No.:65296-08-4
Molecular Formula:C7H14 N2 O2
Molecular Weight:158.2
Hs Code.:
DSSTox Substance ID:DTXSID00421276

Synonyms:DTXSID00421276;65296-08-4;Ethyl (2E)-2-(dimethylhydrazinylidene)propanoate

Suppliers and Price of Ethyl (2E)-2-(dimethylhydrazinylidene)propanoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of Ethyl (2E)-2-(dimethylhydrazinylidene)propanoate

Chemical Property:

Vapor Pressure:0.446mmHg at 25°C
Boiling Point:194.2°Cat760mmHg
Flash Point:71.3°C
Density:0.98g/cm³
XLogP3:1.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:158.105527694
Heavy Atom Count:11
Complexity:164

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C(=NN(C)C)C
Isomeric SMILES:CCOC(=O)/C(=N/N(C)C)/C

Technology Process of Ethyl (2E)-2-(dimethylhydrazinylidene)propanoate

There total 1 articles about Ethyl (2E)-2-(dimethylhydrazinylidene)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 617-35-6
2-oxo-propionic acid ethyl ester

: 57-14-7
N,N-Dimethylhydrazine

: 65296-08-4
ethyl α-(N,N-dimethylhydrazono)-propionate

Guidance literature:: In dichloromethane; at 70 ℃;
DOI:10.1016/0040-4020(96)00940-4

Reference yield:

: 65296-08-4
ethyl α-(N,N-dimethylhydrazono)-propionate

: 617-35-6
2-oxo-propionic acid ethyl ester

Guidance literature:: With [hydroxy(tosyloxy)iodo]benzene; In chloroform-d1; Ambient temperature;
DOI:10.1016/0040-4020(96)00940-4

Reference yield:

: 65296-08-4
ethyl α-(N,N-dimethylhydrazono)-propionate

: 184579-16-6
2-Hydroxy-2-phenylazo-propionic acid ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent Spectr_. / HTIB / CDCl₃ / Ambient temperature

2: CH₂Cl₂

3: 93 percent / CH₂Cl₂ / 2 h

4: 86 percent / 2-t-butyl-1,1,3,3-tetramethyl guanidine / ethanol / 1 h / Ambient temperature

With [hydroxy(tosyloxy)iodo]benzene; N,N,N′,N′-tetramethyl-N″-tert-butylguanidine; In chloroform-d1; ethanol; dichloromethane;
DOI:10.1016/0040-4020(96)00940-4