Benzamide, 4-[(1E)-3-[[3'-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-2',4'-dimethyl[ 1,1'-biphenyl]-3-yl]amino]-3-oxo-1-propenyl]-N-methyl-

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Chemical Name:Benzamide, 4-[(1E)-3-[[3'-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-2',4'-dimethyl[ 1,1'-biphenyl]-3-yl]amino]-3-oxo-1-propenyl]-N-methyl-
CAS No.:189269-07-6
Molecular Formula:C42H44N2O3Si
Molecular Weight:652.908
Hs Code.:

Synonyms:

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Chemical Property of Benzamide, 4-[(1E)-3-[[3'-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-2',4'-dimethyl[ 1,1'-biphenyl]-3-yl]amino]-3-oxo-1-propenyl]-N-methyl-

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Technology Process of Benzamide, 4-[(1E)-3-[[3'-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-2',4'-dimethyl[ 1,1'-biphenyl]-3-yl]amino]-3-oxo-1-propenyl]-N-methyl-

There total 3 articles about Benzamide, 4-[(1E)-3-[[3'-[[[(1,1-dimethylethyl)diphenylsilyl]oxy]methyl]-2',4'-dimethyl[ 1,1'-biphenyl]-3-yl]amino]-3-oxo-1-propenyl]-N-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 189269-03-2
3-(3-aminophenyl)-1-tert-butyldiphenylsilyloxymethyl-2,6-dimethylbenzene

: 179627-11-3
4-(methylcarbamoyl)cinnamic acid

: 189269-07-6
1-tert-Butyldiphenylsilyloxymethyl-2,6-dimethyl-3-[3-[4-(methylcarbamoyl)cinnamoylamino]phenyl]benzene

Guidance literature:: With WSCD*HCl; benzotriazol-1-ol; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 2.5h;
DOI:10.1021/jm980330i

Reference yield:

: 1-tert-butyldiphenylsilyloxymethyl-2,6-dimethyl-3-bromobenzene

: 189269-07-6
1-tert-Butyldiphenylsilyloxymethyl-2,6-dimethyl-3-[3-[4-(methylcarbamoyl)cinnamoylamino]phenyl]benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 34.1 percent / tetrakis(triphenylphosphine)palladium⁽⁰⁾, 2 M aq. Na₂CO₃ / methanol; toluene / 5 h / 80 °C

2: HOBt, WSCD*HCl / dimethylformamide / 2.5 h / 0 - 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; WSCD*HCl; sodium carbonate; benzotriazol-1-ol; In methanol; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm980330i

Reference yield:

: bis[3-(dihydroxyboranyl)benzeneaminium] sulfate

: 189269-07-6
1-tert-Butyldiphenylsilyloxymethyl-2,6-dimethyl-3-[3-[4-(methylcarbamoyl)cinnamoylamino]phenyl]benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 34.1 percent / tetrakis(triphenylphosphine)palladium⁽⁰⁾, 2 M aq. Na₂CO₃ / methanol; toluene / 5 h / 80 °C

2: HOBt, WSCD*HCl / dimethylformamide / 2.5 h / 0 - 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; WSCD*HCl; sodium carbonate; benzotriazol-1-ol; In methanol; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm980330i