2H-1,3-Oxazine-2,4(3H)-dione, dihydro-3-(phenylamino)-

Base Information

Chemical Name:2H-1,3-Oxazine-2,4(3H)-dione, dihydro-3-(phenylamino)-
CAS No.:189322-90-5
Molecular Formula:C10H10N2O3
Molecular Weight:206.201
Hs Code.:
DSSTox Substance ID:DTXSID80450882
Nikkaji Number:J826.306J

Synonyms:189322-90-5;2H-1,3-Oxazine-2,4(3H)-dione, dihydro-3-(phenylamino)-;DTXSID80450882;3-(Phenylamino)dihydro-2H-1,3-oxazine-2,4(3H)-dione

Suppliers and Price of 2H-1,3-Oxazine-2,4(3H)-dione, dihydro-3-(phenylamino)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 2H-1,3-Oxazine-2,4(3H)-dione, dihydro-3-(phenylamino)-

Chemical Property:

XLogP3:1.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:206.06914219
Heavy Atom Count:15
Complexity:261

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1COC(=O)N(C1=O)NC2=CC=CC=C2

Technology Process of 2H-1,3-Oxazine-2,4(3H)-dione, dihydro-3-(phenylamino)-

There total 4 articles about 2H-1,3-Oxazine-2,4(3H)-dione, dihydro-3-(phenylamino)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 189322-86-9
3-Hydroxy-3-phenylazo-dihydro-furan-2-one

: 189322-90-5
3-Phenylamino-[1,3]oxazinane-2,4-dione

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; Ambient temperature;
DOI:10.1039/a607830c

Reference yield: 18.0%

: 368-39-8
triethyloxonium fluoroborate

: 189322-86-9
3-Hydroxy-3-phenylazo-dihydro-furan-2-one

: 189322-90-5
3-Phenylamino-[1,3]oxazinane-2,4-dione

: 3-(Ethyl-phenyl-amino)-[1,3]oxazinane-2,4-dione

: N'-Ethyl-N-(3-hydroxy-propionyl)-N'-phenyl-hydrazinecarboxylic acid ethyl ester

Guidance literature:: In dichloromethane;
DOI:10.1039/a607830c

Reference yield:

: 100-34-5
benzene diazonium chloride

: 189322-90-5
3-Phenylamino-[1,3]oxazinane-2,4-dione

Guidance literature:: Multi-step reaction with 4 steps

1: 92 percent / aq. NaOH

2: 98 percent / bis(trifluoroacetoxy)iodobenzene

3: aq. Na₂CO₃

4: 95 percent / Et₂O*BF₃ / CH₂Cl₂ / Ambient temperature

With sodium hydroxide; boron trifluoride diethyl etherate; sodium carbonate; bis-[(trifluoroacetoxy)iodo]benzene; In dichloromethane;
DOI:10.1039/a607830c