3-(2-methoxyethoxy)prop-1-ene

Base Information

• Chemical Name: 3-(2-methoxyethoxy)prop-1-ene
• CAS No.: 10021-77-9
• Molecular Formula: C4H4 Cl2 O2 S2
• Molecular Weight: 219.11
• Hs Code.: 2930909090
• Mol file: 10021-77-9.mol

Synonyms:Acetylchloride, dithiodi- (7CI,8CI); Dithiodiacetyl chloride; Dithiodiacetyldichloride; Dithiodiglycolyl chloride

Chemical Property of 3-(2-methoxyethoxy)prop-1-ene

Chemical Property:

• PSA: 84.74000
• LogP: 1.89860

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-(2-methoxyethoxy)prop-1-ene

There total 1 articles about 3-(2-methoxyethoxy)prop-1-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

disulfanediyldiacetic acid (505-73-7) → 2,2'-disulfanediyldiacetylchloride (10021-77-9)

Guidance literature:

With thionyl chloride; N,N-dimethyl-formamide; In dichloromethane; at 20 ℃; for 0.5h;

Reference yield: 89.0%

2,2'-disulfanediyldiacetylchloride (10021-77-9) + 4-bromo-aniline (106-40-1) → 2,2’-dithiobis(N-(4-bromophenyl)acetamide) (94029-36-4)

Guidance literature:

In dichloromethane; for 2h;

Reference yield: 75.0%

2,2'-disulfanediyldiacetylchloride (10021-77-9) + 2-(3,4-dimethoxyphenyl)-ethylamine (120-20-7) → disulfure de β,β'-propionylhomoveratrylamine (89042-60-4)

Guidance literature:

In diethyl ether; for 1h; Ambient temperature;

upstream raw materials:

disulfanediyldiacetic acid

Downstream raw materials:

N-phenyl-mercaptoacetamide disulfide

methyl 4-(methoxysulfinyl)phenyl 2,2'-dithiodiacetate

bis<4-(methoxysulfinyl)phenyl> 2,2'-dithiodiacetate

bis<2-(methoxysulfinyl)-4,6-dichlorophenyl> 2,2'-dithiodiacetate

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