1-Isoquinolinecarboxaldehyde, 3-phenyl-

Base Information

Chemical Name:1-Isoquinolinecarboxaldehyde, 3-phenyl-
CAS No.:189816-06-6
Molecular Formula:C16H11NO
Molecular Weight:233.269
Hs Code.:

Synonyms:

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Chemical Property of 1-Isoquinolinecarboxaldehyde, 3-phenyl-

Chemical Property:

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Technology Process of 1-Isoquinolinecarboxaldehyde, 3-phenyl-

There total 12 articles about 1-Isoquinolinecarboxaldehyde, 3-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1721-96-6
1-methyl-3-phenylisoquinoline

: 189816-06-6
3-Phenyl-isoquinoline-1-carbaldehyde

Guidance literature:: With selenium(IV) oxide; In 1,4-dioxane; at 102 ℃; for 3h; Schlenk technique; Sealed tube;
DOI:10.1021/acs.orglett.1c01237

Reference yield: 75.0%

: (3-phenylisoquinolin-1-yl)methanol

: 189816-06-6
3-Phenyl-isoquinoline-1-carbaldehyde

Guidance literature:: With sulfur trioxide pyridine complex; triethylamine; In dimethyl sulfoxide; at 20 ℃; for 10h;
DOI:10.1016/j.tetlet.2019.151287

Reference yield:

: C₁₄H₁₈O₃

: 189816-06-6
3-Phenyl-isoquinoline-1-carbaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: ammonium hydroxide / water; acetonitrile / 12 h / 70 °C

2: pyridine / dichloromethane / 1 h / 0 °C

3: methanesulfonic acid(2-dicyclohexylphosphino-2′,4′,6′-triisopropyl-1,1′-biphenyl)[2-(2′-amino-1,1′-biphenyl)]palladium(II); potassium phosphate / tetrahydrofuran / 2 h / 40 °C

4: selenium(IV) oxide / 1,4-dioxane / 2 h / 110 °C

With pyridine; selenium(IV) oxide; ammonium hydroxide; potassium phosphate; methanesulfonic acid(2-dicyclohexylphosphino-2′,4′,6′-triisopropyl-1,1′-biphenyl)[2-(2′-amino-1,1′-biphenyl)]palladium(II); In tetrahydrofuran; 1,4-dioxane; dichloromethane; water; acetonitrile; 3: |Suzuki Coupling;
DOI:10.1021/acscatal.0c00211