SODIUM, 4-METHYL-PIPERAZINE-1-CARBODITHIOATE

Base Information

• Chemical Name: SODIUM, 4-METHYL-PIPERAZINE-1-CARBODITHIOATE
• CAS No.: 5712-49-2
• Molecular Formula: C6H11N2NaS2
• Molecular Weight: 198.289
• Mol file: 5712-49-2.mol

Synonyms:sodium 4-methylpiperazine-1-carbodithioate;4-methyl-piperazine-1-carbodithioic acid,sodium salt;BB_SC-0260;4-MPipzcdtNa;sodium 4-methylpiperidyldithiocarbamate;4-Methyl-1-piperazinecarbodithioic acid sodium salt;1-Piperazinecarbodithioic acid,4-methyl-,sodium salt;sodium 4-methyl-1-piperazinecarbodithioate;

Chemical Property of SODIUM, 4-METHYL-PIPERAZINE-1-CARBODITHIOATE

Chemical Property:

• Vapor Pressure: 0.0574mmHg at 25°C
• Boiling Point: 233°Cat760mmHg
• Flash Point: 94.7°C
• PSA: 38.57000
• Density: g/cm³
• LogP: -0.05860

Purity/Quality:

99% ^*data from raw suppliers

Sodium 4-methylpiperazine-1-carbodithioate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of SODIUM, 4-METHYL-PIPERAZINE-1-CARBODITHIOATE

There total 2 articles about SODIUM, 4-METHYL-PIPERAZINE-1-CARBODITHIOATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-methyl-piperazine (109-01-3) + carbon disulfide (75-15-0,12122-00-8) → sodium 4-methyl-1-piperazinecarbodithioate (5712-49-2)

Guidance literature:

With sodium hydroxide; In diethyl ether; for 4h;

DOI:10.1016/0022-2860(80)85202-1

Reference yield:

1-methyl-piperazine (109-01-3) + 1-(2-chloroethyl)-2-methyl-5-nitro-1H-imidazole (13182-81-5) → 2-(2-methyl-5-nitro-1H-imidazol-1-yl)ethyl 4-methylpiperazine-1-carbodithioate (52187-06-1) + sodium 4-methyl-1-piperazinecarbodithioate (5712-49-2)

Guidance literature:

With sodium iodide; In N-methyl-acetamide;

Reference yield: 89.0%

2-chloro-N-(3,4-difluorophenyl)acetamide (76778-13-7) + sodium 4-methyl-1-piperazinecarbodithioate (5712-49-2) → C14H17F2N3OS2

Guidance literature:

In acetone; for 2h; Reflux;

DOI:10.1080/10426507.2016.1259228

upstream raw materials:

1-methyl-piperazine

carbon disulfide

1-(2-chloroethyl)-2-methyl-5-nitro-1H-imidazole

Downstream raw materials:

((CH₃)3CC₆H₄)2Sn(S₂CN(CH₂)4N(CH₃))2

bis(4-methylpiperazinedithiocarbamato)bis(p-biphenyl)tin(IV)

bis-N-methylpiperazine dithiocarbamato-di-p-tolyltin(IV)

(C₆H₅)3SnSC(S)NC₄H₈NCH₃