bis-N-methylpiperazine dithiocarbamato-di-p-tolyltin(IV)

Base Information

• Chemical Name: bis-N-methylpiperazine dithiocarbamato-di-p-tolyltin(IV)
• CAS No.: 81641-61-4
• Molecular Formula: C₂₆H₃₆N₄S₄Sn
• Molecular Weight: 651.573
• Mol file: 81641-61-4.mol

Synonyms:

Chemical Property of bis-N-methylpiperazine dithiocarbamato-di-p-tolyltin(IV)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of bis-N-methylpiperazine dithiocarbamato-di-p-tolyltin(IV)

There total 2 articles about bis-N-methylpiperazine dithiocarbamato-di-p-tolyltin(IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tetra(p-tolyl)tin (6746-22-1) → bis-N-methylpiperazine dithiocarbamato-di-p-tolyltin(IV) (81641-61-4)

Guidance literature:

Multi-step reaction with 2 steps

2: acetone

In acetone;

Reference yield:

di(p-tolyl)tin dichloride (32538-29-7) + sodium 4-methyl-1-piperazinecarbodithioate (5712-49-2) → bis-N-methylpiperazine dithiocarbamato-di-p-tolyltin(IV) (81641-61-4)

Guidance literature:

In acetone; byproducts: NaCl; mixed of educts in stoich. ratio at room temp., dry acetone, stirred, reflux for 1/2 h, kept at room temp for 1/2 h; filtered, filtrate evapd. under vac., recrystd. from CH2Cl2 and petroleum ether, elem. anal.;

upstream raw materials:

di(p-tolyl)tin dichloride

sodium 4-methyl-1-piperazinecarbodithioate

tetra(p-tolyl)tin