(2,5-Bis(1-aziridinyl)-3,6-dioxo-1,4-cyclohexadiene-1,4-diyl)biscarbam ic acid, dibutyl ester

Base Information

Chemical Name:(2,5-Bis(1-aziridinyl)-3,6-dioxo-1,4-cyclohexadiene-1,4-diyl)biscarbam ic acid, dibutyl ester
CAS No.:125671-99-0
Molecular Formula:C20H28 N4 O6
Molecular Weight:420.4595
Hs Code.:
Mol file:125671-99-0.mol

Synonyms:Carbamicacid, [2,5-bis(1-aziridinyl)-3,6-dioxo-1,4-cyclohexadiene-1,4-diyl]bis-,dibutyl ester (9CI)

Suppliers and Price of (2,5-Bis(1-aziridinyl)-3,6-dioxo-1,4-cyclohexadiene-1,4-diyl)biscarbam ic acid, dibutyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of (2,5-Bis(1-aziridinyl)-3,6-dioxo-1,4-cyclohexadiene-1,4-diyl)biscarbam ic acid, dibutyl ester

Chemical Property:

Vapor Pressure:1.1E-10mmHg at 25°C
Boiling Point:514.2°Cat760mmHg
Flash Point:264.8°C
PSA：123.80000
Density:1.33g/cm³
LogP:1.52980

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of (2,5-Bis(1-aziridinyl)-3,6-dioxo-1,4-cyclohexadiene-1,4-diyl)biscarbam ic acid, dibutyl ester

There total 6 articles about (2,5-Bis(1-aziridinyl)-3,6-dioxo-1,4-cyclohexadiene-1,4-diyl)biscarbam ic acid, dibutyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 151-56-4,9002-98-6
ethyleneimine

: 125659-87-2
(4-Butoxycarbonylamino-2,5-dichloro-3,6-dioxo-cyclohexa-1,4-dienyl)-carbamic acid butyl ester

: 125671-99-0
(2,5-Bis-aziridin-1-yl-4-butoxycarbonylamino-3,6-dioxo-cyclohexa-1,4-dienyl)-carbamic acid butyl ester

Guidance literature:: With triethylamine; In tetrahydrofuran; for 10h; Ambient temperature;
DOI:10.1055/s-1989-27348

Reference yield:

: 3908-48-3
2,5-diamino-3,6-dichloro-1,4-benzoquinone

: 125671-99-0
(2,5-Bis-aziridin-1-yl-4-butoxycarbonylamino-3,6-dioxo-cyclohexa-1,4-dienyl)-carbamic acid butyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: Na₂S₂O₄ / H₂O; cyclohexane / 0.33 h / 25 °C

2: H₂O; cyclohexane / 4 h / 25 °C

3: FeCl₃, aq. HCl / 3 h / 25 °C

4: 92 percent / conc. H₂SO₄ / 8 h / Heating

5: 81 percent / Et₃N / tetrahydrofuran / 10 h / Ambient temperature

With hydrogenchloride; sodium dithionite; sulfuric acid; iron(III) chloride; triethylamine; In tetrahydrofuran; cyclohexane; water;
DOI:10.1055/s-1989-27348

Reference yield:

: 24118-25-0
3,6-diamino-2,5-dichloro-1,4-hydroquinone

: 125671-99-0
(2,5-Bis-aziridin-1-yl-4-butoxycarbonylamino-3,6-dioxo-cyclohexa-1,4-dienyl)-carbamic acid butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: H₂O; cyclohexane / 4 h / 25 °C

2: FeCl₃, aq. HCl / 3 h / 25 °C

3: 92 percent / conc. H₂SO₄ / 8 h / Heating

4: 81 percent / Et₃N / tetrahydrofuran / 10 h / Ambient temperature

With hydrogenchloride; sulfuric acid; iron(III) chloride; triethylamine; In tetrahydrofuran; cyclohexane; water;
DOI:10.1055/s-1989-27348