(4-Butoxycarbonylamino-2,5-dichloro-3,6-dioxo-cyclohexa-1,4-dienyl)-carbamic acid butyl ester

Base Information

Chemical Name:(4-Butoxycarbonylamino-2,5-dichloro-3,6-dioxo-cyclohexa-1,4-dienyl)-carbamic acid butyl ester
CAS No.:125659-87-2
Molecular Formula:C₁₆H₂₀Cl₂N₂O₆
Molecular Weight:407.251
Hs Code.:

Synonyms:(4-Butoxycarbonylamino-2,5-dichloro-3,6-dioxo-cyclohexa-1,4-dienyl)-carbamic acid butyl ester

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Chemical Property of (4-Butoxycarbonylamino-2,5-dichloro-3,6-dioxo-cyclohexa-1,4-dienyl)-carbamic acid butyl ester

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Technology Process of (4-Butoxycarbonylamino-2,5-dichloro-3,6-dioxo-cyclohexa-1,4-dienyl)-carbamic acid butyl ester

There total 5 articles about (4-Butoxycarbonylamino-2,5-dichloro-3,6-dioxo-cyclohexa-1,4-dienyl)-carbamic acid butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 24118-24-9
2,5-dichloro-3,6-bis(methoxycarbonylamino)-1,4-benzoquinone

: 71-36-3
butan-1-ol

: 125659-87-2
(4-Butoxycarbonylamino-2,5-dichloro-3,6-dioxo-cyclohexa-1,4-dienyl)-carbamic acid butyl ester

Guidance literature:: With sulfuric acid; for 8h; Heating;
DOI:10.1055/s-1989-27348

Reference yield:

: 3908-48-3
2,5-diamino-3,6-dichloro-1,4-benzoquinone

: 125659-87-2
(4-Butoxycarbonylamino-2,5-dichloro-3,6-dioxo-cyclohexa-1,4-dienyl)-carbamic acid butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: Na₂S₂O₄ / H₂O; cyclohexane / 0.33 h / 25 °C

2: H₂O; cyclohexane / 4 h / 25 °C

3: FeCl₃, aq. HCl / 3 h / 25 °C

4: 92 percent / conc. H₂SO₄ / 8 h / Heating

With hydrogenchloride; sodium dithionite; sulfuric acid; iron(III) chloride; In cyclohexane; water;
DOI:10.1055/s-1989-27348

Reference yield:

: 24118-25-0
3,6-diamino-2,5-dichloro-1,4-hydroquinone

: 125659-87-2
(4-Butoxycarbonylamino-2,5-dichloro-3,6-dioxo-cyclohexa-1,4-dienyl)-carbamic acid butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: H₂O; cyclohexane / 4 h / 25 °C

2: FeCl₃, aq. HCl / 3 h / 25 °C

3: 92 percent / conc. H₂SO₄ / 8 h / Heating

With hydrogenchloride; sulfuric acid; iron(III) chloride; In cyclohexane; water;
DOI:10.1055/s-1989-27348