1,3-Diazaspiro[4.5]decane-1,3-dicarboxylic acid, 8-[[(1,1-dimethylethoxy)carbonyl](phenylmethyl)amino]-2,4-dioxo-, bis(1,1-dimethylethyl) ester

Base Information

Chemical Name:1,3-Diazaspiro[4.5]decane-1,3-dicarboxylic acid, 8-[[(1,1-dimethylethoxy)carbonyl](phenylmethyl)amino]-2,4-dioxo-, bis(1,1-dimethylethyl) ester
CAS No.:192373-17-4
Molecular Formula:C₃₀H₄₃N₃O₈
Molecular Weight:573.687
Hs Code.:

1,3-Diazaspiro[4.5]decane-1,3-dicarboxylic acid,
8-[[(1,1-dimethylethoxy)carbonyl](phenylmethyl)amino]-2,4-dioxo-,
bis(1,1-dimethylethyl) ester

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Chemical Property of 1,3-Diazaspiro[4.5]decane-1,3-dicarboxylic acid, 8-[[(1,1-dimethylethoxy)carbonyl](phenylmethyl)amino]-2,4-dioxo-, bis(1,1-dimethylethyl) ester

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Technology Process of 1,3-Diazaspiro[4.5]decane-1,3-dicarboxylic acid, 8-[[(1,1-dimethylethoxy)carbonyl](phenylmethyl)amino]-2,4-dioxo-, bis(1,1-dimethylethyl) ester

There total 4 articles about 1,3-Diazaspiro[4.5]decane-1,3-dicarboxylic acid, 8-[[(1,1-dimethylethoxy)carbonyl](phenylmethyl)amino]-2,4-dioxo-, bis(1,1-dimethylethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 131511-13-2
4-(N-benzylamino)cyclohexanone ethylene acetal

: 192373-17-4
8-(Benzyl-tert-butoxycarbonyl-amino)-2,4-dioxo-1,3-diaza-spiro[4.5]decane-1,3-dicarboxylic acid di-tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 20percent trifluoroacetic acid/water / tetrahydrofuran / 24 h / Heating

2: Et₃N, DMAP / tetrahydrofuran

4: DMAP

With dmap; water; triethylamine; trifluoroacetic acid; In tetrahydrofuran;
DOI:10.1016/S0040-4039(97)00822-8

Reference yield:

: 142009-99-2
4-(benzylamino)cyclohexane-1-one

: 192373-17-4
8-(Benzyl-tert-butoxycarbonyl-amino)-2,4-dioxo-1,3-diaza-spiro[4.5]decane-1,3-dicarboxylic acid di-tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N, DMAP / tetrahydrofuran

3: DMAP

With dmap; triethylamine; In tetrahydrofuran;
DOI:10.1016/S0040-4039(97)00822-8

Reference yield:

: 100-46-9
benzylamine

: 192373-17-4
8-(Benzyl-tert-butoxycarbonyl-amino)-2,4-dioxo-1,3-diaza-spiro[4.5]decane-1,3-dicarboxylic acid di-tert-butyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: sodium triacetoxyborohydride, acetic acid / 1,2-dichloro-ethane

2: 20percent trifluoroacetic acid/water / tetrahydrofuran / 24 h / Heating

3: Et₃N, DMAP / tetrahydrofuran

5: DMAP

With dmap; water; sodium tris(acetoxy)borohydride; acetic acid; triethylamine; trifluoroacetic acid; In tetrahydrofuran; 1,2-dichloro-ethane;
DOI:10.1016/S0040-4039(97)00822-8