Hydroveratroin

Base Information

• Chemical Name: Hydroveratroin
• CAS No.: 4433-66-3
• Molecular Formula: C₁₈H₂₂O₆
• Molecular Weight: 334.369
• Mol file: 4433-66-3.mol

Synonyms:

Chemical Property of Hydroveratroin

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Hydroveratroin

There total 15 articles about Hydroveratroin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

3,4-dimethoxy-benzaldehyde (120-14-9) → bis-(3,4-dimethoxyphenyl)-1,2-ethanediol (4433-66-3)

Guidance literature:

With iodine; magnesium; In methanol; at 20 ℃; for 0.5h;

Reference yield: 78.0%

3,3',4,4'-tetramethoxybenzoin (5653-60-1) → meso-hydroveratroin (5565-49-1) + (+/-)-hydroveratroin (4433-66-3,5565-49-1,67042-32-4,131349-65-0)

Guidance literature:

With dimethylsulfide borane complex; In tetrahydrofuran; for 2h; Ambient temperature;

Reference yield: 69.0%

3,4-dimethoxy-benzaldehyde (120-14-9) → 3,4,3',4'-Tetramethoxystilben (18513-98-9) + meso-hydroveratroin (5565-49-1) + (+/-)-hydroveratroin (4433-66-3,5565-49-1,67042-32-4,131349-65-0)

Guidance literature:

With titanium tetrachloride; zinc; In tetrahydrofuran; for 3h; Yield given; Ambient temperature;

upstream raw materials:

3,4-dimethoxy-benzaldehyde

benzaldehyde

(+/-)-hydroveratroin

3,3',4,4'-tetramethoxybenzoin

Downstream raw materials:

(S:S)-1,2-bis-(3,4-dimethoxy-phenyl)-ethanediol-(1,2)

(R:R)-1,2-bis-(3,4-dimethoxy-phenyl)-ethanediol-(1,2)

2-(3,4-dimethoxyphenyl)-4,5-diphenyl-1H-imidazole

Refernces

• 1、 Duan, Xin-Fang,Feng, Jian-Xia,Zi, Guo-Fu,Zhang, Zhan-Bin. "A convenient synthesis of unsymmetrical pinacols by coupling of structurally similar aromatic aldehydes mediated by low-valent titanium". experimental part. p. 277 - 282. Retrieved 2009/06/24.
• 2、 Khurana, Jitender M.,Bansal, Geeti,Kukreja, Gagan,Pandey, Ravi R.. "Pinacol Formation and Reduction of Aromatic Carbonyls with Magnesium-Methanol at Ambient Temperature". . p. 1365 - 1371. Retrieved 2007/10/03.