2,2'-Bipyridine, 4,4'-dimethyl-6,6'-diphenyl-

Base Information

Chemical Name:2,2'-Bipyridine, 4,4'-dimethyl-6,6'-diphenyl-
CAS No.:192863-71-1
Molecular Formula:C24H20N2
Molecular Weight:336.436
Hs Code.:
DSSTox Substance ID:DTXSID90478532
Nikkaji Number:J1.063.245E
Wikidata:Q82311990

Synonyms:2,2'-Bipyridine, 4,4'-dimethyl-6,6'-diphenyl-;192863-71-1;DTXSID90478532

Suppliers and Price of 2,2'-Bipyridine, 4,4'-dimethyl-6,6'-diphenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2'-Bipyridine, 4,4'-dimethyl-6,6'-diphenyl-

Chemical Property:

XLogP3:5.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:336.162648646
Heavy Atom Count:26
Complexity:384

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=NC(=C1)C2=CC(=CC(=N2)C3=CC=CC=C3)C)C4=CC=CC=C4

Technology Process of 2,2'-Bipyridine, 4,4'-dimethyl-6,6'-diphenyl-

There total 2 articles about 2,2'-Bipyridine, 4,4'-dimethyl-6,6'-diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1,4,4'-trimethyl-6,6'-diphenyl-2,2'-bipyridinium triflate

: 192863-71-1
4,4’-dimethyl-6,6’-diphenyl-2,2’-bipyridine

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; In N,N-dimethyl-formamide; for 2h; Heating;
DOI:10.1002/ejic.200400418

Reference yield: 20.0%

: 1134-35-6
4,4'-dimethyl-2,2'-bipyridines

: 591-51-5
phenyllithium

: 192863-71-1
4,4’-dimethyl-6,6’-diphenyl-2,2’-bipyridine

Guidance literature:: With manganese(IV) oxide; In toluene;
DOI:10.1016/S0040-4039(97)00896-4

Reference yield: 81.0%

: 17084-13-8
potassium hexafluorophosphate

: cis-dichloridobis(1,10-phenanthroline)ruthenium(II)

: 192863-71-1
4,4’-dimethyl-6,6’-diphenyl-2,2’-bipyridine

: [Ru(1,10-phenanthroline)(4,4'-dimethyl-6,6'-diphenyl-2,2'-bipyridine)](PF₆)2

Guidance literature:: In ethylene glycol; Ar atmosphere, refluc of soln. of Ru complex and bipyridine (3 h), cooling to room temp., addn. of satd. aq. K(PF6); filtration, washing (water, Et2O), drying, chromy. (silica gel, CH2Cl2/MeOH (0-2%));
DOI:10.1002/(sici)1099-0682(199903)1999:3<383::aid-ejic383>3.0.co;2-9