Benzene, [3-(2-iodoethoxy)-1-propynyl]-

Base Information

Chemical Name:Benzene, [3-(2-iodoethoxy)-1-propynyl]-
CAS No.:193091-57-5
Molecular Formula:C11H11IO
Molecular Weight:286.112
Hs Code.:
DSSTox Substance ID:DTXSID10453169
Nikkaji Number:J1.453.038J
Wikidata:Q82274220
Mol file:193091-57-5.mol

Synonyms:Benzene, [3-(2-iodoethoxy)-1-propynyl]-;193091-57-5;DTXSID10453169;(3-Phenyl-2-propynyl)(2-iodoethyl) ether

Suppliers and Price of Benzene, [3-(2-iodoethoxy)-1-propynyl]-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzene, [3-(2-iodoethoxy)-1-propynyl]-

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:285.98546
Heavy Atom Count:13
Complexity:183

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)C#CCOCCI

Technology Process of Benzene, [3-(2-iodoethoxy)-1-propynyl]-

There total 3 articles about Benzene, [3-(2-iodoethoxy)-1-propynyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 99522-44-8
2-((3-phenylprop-2-yn-1-yl)oxy)ethanol

: 193091-57-5
2-iodoethyl 3-phenylpropynyl ether

Guidance literature:: With iodine; triphenylphosphine; In pyridine; dichloromethane; at 0 ℃; for 1h;
DOI:10.1016/S0040-4020(00)01007-3

Reference yield:

: 1504-58-1
3-Phenyl-2-propyn-1-ol

: 193091-57-5
2-iodoethyl 3-phenylpropynyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 1.57 g / PBr₃ / diethyl ether; pyridine / 4 h / 0 °C

2: 94 percent / NaH; HMPA / tetrahydrofuran / 6 h / 0 - 20 °C

3: 91 percent / PPh₃; I₂ / CH₂Cl₂; pyridine / 1 h / 0 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; iodine; phosphorus tribromide; sodium hydride; triphenylphosphine; In tetrahydrofuran; pyridine; diethyl ether; dichloromethane;
DOI:10.1016/S0040-4020(00)01007-3

Reference yield:

: 1794-48-5
1-bromo-3-phenylprop-2-yne

: 193091-57-5
2-iodoethyl 3-phenylpropynyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / NaH; HMPA / tetrahydrofuran / 6 h / 0 - 20 °C

2: 91 percent / PPh₃; I₂ / CH₂Cl₂; pyridine / 1 h / 0 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; iodine; sodium hydride; triphenylphosphine; In tetrahydrofuran; pyridine; dichloromethane;
DOI:10.1016/S0040-4020(00)01007-3