Thiourea, N,N''-[(5-bromo-1,3-phenylene)bis(methylene)]bis[N'-butyl-

Base Information

Chemical Name:Thiourea, N,N''-[(5-bromo-1,3-phenylene)bis(methylene)]bis[N'-butyl-
CAS No.:193606-88-1
Molecular Formula:C₁₈H₂₉BrN₄S₂
Molecular Weight:445.491
Hs Code.:
DSSTox Substance ID:DTXSID30441280
Nikkaji Number:J863.764D
Wikidata:Q82257990
Mol file:193606-88-1.mol

Synonyms:Thiourea, N,N''-[(5-bromo-1,3-phenylene)bis(methylene)]bis[N'-butyl-;193606-88-1;DTXSID30441280;1,1'-(5-Bromo-1,3-xylylene)bis(3-butylthiourea)

Suppliers and Price of Thiourea, N,N''-[(5-bromo-1,3-phenylene)bis(methylene)]bis[N'-butyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 1 raw suppliers

Chemical Property of Thiourea, N,N''-[(5-bromo-1,3-phenylene)bis(methylene)]bis[N'-butyl-

Chemical Property:

XLogP3:4.2
Hydrogen Bond Donor Count:4
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:10
Exact Mass:444.10170
Heavy Atom Count:25
Complexity:361

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCNC(=S)NCC1=CC(=CC(=C1)Br)CNC(=S)NCCCC

Technology Process of Thiourea, N,N''-[(5-bromo-1,3-phenylene)bis(methylene)]bis[N'-butyl-

There total 3 articles about Thiourea, N,N''-[(5-bromo-1,3-phenylene)bis(methylene)]bis[N'-butyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 592-82-5
butyl isothiocyanate

: 214400-65-4
1,3-bis(aminomethyl)-5-bromobenzene

: 193606-88-1
1-{3-Bromo-5-[(3-butyl-thioureido)-methyl]-benzyl}-3-butyl-thiourea

Guidance literature:: In tetrahydrofuran; for 1h; Heating;
DOI:10.1021/jo980441p

Reference yield:

: 51760-23-7
1-bromo-3,5-bis(bromomethyl)benzene

: 193606-88-1
1-{3-Bromo-5-[(3-butyl-thioureido)-methyl]-benzyl}-3-butyl-thiourea

Guidance literature:: Multi-step reaction with 3 steps

1: dimethylformamide / 4 h / 90 °C

2: NH₂NH₂*H₂O / ethanol / 1 h / Heating

3: 72 percent / tetrahydrofuran / 1 h / Heating

With hydrazine hydrate; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jo980441p

Reference yield:

: 212311-96-1
5-bromo-1,3-bis(phthalimidomethyl)benzene

: 193606-88-1
1-{3-Bromo-5-[(3-butyl-thioureido)-methyl]-benzyl}-3-butyl-thiourea

Guidance literature:: Multi-step reaction with 2 steps

1: NH₂NH₂*H₂O / ethanol / 1 h / Heating

2: 72 percent / tetrahydrofuran / 1 h / Heating

With hydrazine hydrate; In tetrahydrofuran; ethanol;
DOI:10.1021/jo980441p