2,5-Piperazinedione, 1-[(4-methoxyphenyl)methyl]-4-methyl-3-(phenylmethyl)-6-[(2,4,5-trimeth oxy-3-methylphenyl)methylene]-, (Z)-

Base Information

• Chemical Name: 2,5-Piperazinedione, 1-[(4-methoxyphenyl)methyl]-4-methyl-3-(phenylmethyl)-6-[(2,4,5-trimeth oxy-3-methylphenyl)methylene]-, (Z)-
• CAS No.: 193686-34-9
• Molecular Formula: C31H34N2O6
• Molecular Weight: 530.621
• Mol file: 193686-34-9.mol

Synonyms:

Chemical Property of 2,5-Piperazinedione, 1-[(4-methoxyphenyl)methyl]-4-methyl-3-(phenylmethyl)-6-[(2,4,5-trimeth oxy-3-methylphenyl)methylene]-, (Z)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,5-Piperazinedione, 1-[(4-methoxyphenyl)methyl]-4-methyl-3-(phenylmethyl)-6-[(2,4,5-trimeth oxy-3-methylphenyl)methylene]-, (Z)-

There total 1 articles about 2,5-Piperazinedione, 1-[(4-methoxyphenyl)methyl]-4-methyl-3-(phenylmethyl)-6-[(2,4,5-trimeth oxy-3-methylphenyl)methylene]-, (Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl bromide (100-39-0) + (Z)-4-(4-methoxyphenylmethyl)-1-methyl-3-(2,4,5-trimethoxy-3-methylphenylmethylene)-2,5-piperazinedione (120040-37-1) → (Z)-6-benzyl-4-(4-methoxybenzyl)-3-(2,4,5-trimethoxy-3-methylbenzylidene)-1-methylpiperazine-2,5-dione (193686-34-9)

Guidance literature:

With sodium hydride; Yield given. Multistep reaction; 1.) THF, 0 deg C, 30 min, 2.) THF, reflux, 3 h;

DOI:10.1248/cpb.45.1120

Reference yield: 83.4%

(Z)-6-benzyl-4-(4-methoxybenzyl)-3-(2,4,5-trimethoxy-3-methylbenzylidene)-1-methylpiperazine-2,5-dione (193686-34-9) → (Z)-6-benzyl-3-(2,4,5-trimethoxy-3-methylbenzylidene)-1-methylpiperazine-2,5-dione

Guidance literature:

With sulfuric acid; In trifluoroacetic acid; for 24h; Ambient temperature;

DOI:10.1248/cpb.45.1120

upstream raw materials:

benzyl bromide

(Z)-4-(4-methoxyphenylmethyl)-1-methyl-3-(2,4,5-trimethoxy-3-methylphenylmethylene)-2,5-piperazinedione