Phosphoric acid, 2-(diethoxyphosphinyl)-1-phenylethenyl diethyl ester, (Z)-

Base Information

Chemical Name:Phosphoric acid, 2-(diethoxyphosphinyl)-1-phenylethenyl diethyl ester, (Z)-
CAS No.:194666-43-8
Molecular Formula:C16H26O7P2
Molecular Weight:392.326
Hs Code.:

Synonyms:

Suppliers and Price of Phosphoric acid, 2-(diethoxyphosphinyl)-1-phenylethenyl diethyl ester, (Z)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Phosphoric acid, 2-(diethoxyphosphinyl)-1-phenylethenyl diethyl ester, (Z)-

Chemical Property:

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Phosphoric acid, 2-(diethoxyphosphinyl)-1-phenylethenyl diethyl ester, (Z)-

There total 1 articles about Phosphoric acid, 2-(diethoxyphosphinyl)-1-phenylethenyl diethyl ester, (Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 70-11-1
α-bromoacetophenone

: 194666-43-8
[(Z)-2-(Diethoxy-phosphoryloxy)-2-phenyl-vinyl]-phosphonic acid diethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene / 12 h / Reflux

2.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -20 °C / Inert atmosphere

2.2: 0.5 h / -20 - 20 °C / Inert atmosphere

With lithium hexamethyldisilazane; In tetrahydrofuran; toluene;
DOI:10.1002/ejoc.201501092