1-(3,4-Dihydro-2-naphthyl)pyrrolidine

Base Information

• Chemical Name: 1-(3,4-Dihydro-2-naphthyl)pyrrolidine
• CAS No.: 21403-95-2
• Molecular Formula: C14H17 N
• Molecular Weight: 199.296
• Hs Code.: 2933990090
• European Community (EC) Number: 244-371-9
• DSSTox Substance ID: DTXSID90175675
• Nikkaji Number: J226.199E
• Wikidata: Q83046005
• Mol file: 21403-95-2.mol

Synonyms:1-(3,4-Dihydro-2-naphthyl)pyrrolidine;21403-95-2;1-(3,4-dihydronaphthalen-2-yl)pyrrolidine;1-(3,4-Dihydro-2-naphthyl)-pyrrolidine;EINECS 244-371-9;SCHEMBL1637987;DTXSID90175675;2-pyrrolidino-3,4-dihydronaphthalene;AKOS015898157;1,2-dihydro-3-pyrrolidinyl-naphthalene;1-(3,4-dihydro-2-napthyl)pyrrolidine;3,4-Dihydronaphthalene, 2-pyrrolidino-;1,2-dihydro- 3-pyrrolidinyl-naphthalene;1-(3,4-dihydronaphthalen-2-yl)-pyrrolidine;1-(3,4-dihydronaphthalene-2-yl)pyrrolidine;FT-0638117;1-(3,4-Dihydro-2-naphthalenyl)pyrrolidine #;1-(3,4-Dihydro-2-naphthyl)pyrrolidine, 97%;Pyrrolidine, 1-(3,4-dihydro-2-naphthalenyl)-;A815314;J-014032

Chemical Property of 1-(3,4-Dihydro-2-naphthyl)pyrrolidine

Chemical Property:

• Vapor Pressure: 0.000184mmHg at 25°C
• Melting Point: 82-84 °C(lit.)
• Boiling Point: 328.9°Cat760mmHg
• Flash Point: 138.7°C
• PSA: 3.24000
• Density: 1.101g/cm³
• LogP: 3.00740
• Storage Temp.: 2-8°C
• XLogP3: 3.3
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 199.136099547
• Heavy Atom Count: 15
• Complexity: 250

Purity/Quality:

97% ^*data from raw suppliers

1-(3,4-Dihydro-2-naphthyl)pyrrolidine 97% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-37/39

MSDS Files:

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: C1CCN(C1)C2=CC3=CC=CC=C3CC2

Technology Process of 1-(3,4-Dihydro-2-naphthyl)pyrrolidine

There total 2 articles about 1-(3,4-Dihydro-2-naphthyl)pyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

pyrrolidine (123-75-1) + 1,2,3,4-tetrahydronaphthalen-2-one (530-93-8) → 1-(3,4-dihydronaphthalene-2-yl)pyrrolidine (21403-95-2)

Guidance literature:

With toluene-4-sulfonic acid; In benzene; for 3h; Heating;

Reference yield:

→ 1-(3,4-dihydronaphthalene-2-yl)pyrrolidine (21403-95-2)

Guidance literature:

DOI:10.1021/ja00885a021 DOI:10.1016/0040-4020(61)80083-5

Reference yield: 73.0%

1-(3,4-dihydronaphthalene-2-yl)pyrrolidine (21403-95-2) + 2-propenamide (79-06-1,12624-24-7,25038-45-3,27754-57-0,33338-03-3,39387-77-4,68247-81-4,9082-06-8,79079-15-5) → 1,4,5,6-tetrahydrobenzoquinolin-3(2H)-one (31951-25-4)

Guidance literature:

at 100 ℃; for 0.5h;

DOI:10.1002/jhet.5570330370

upstream raw materials:

pyrrolidine

1,2,3,4-tetrahydronaphthalen-2-one

Downstream raw materials:

1-methyl-2-tetralone

[1-Indan-1-yl-1-pyrrolidin-1-yl-meth-(Z)-ylidene]-phosphoramidic acid diphenyl ester

((3aS,9bR)-3a-Pyrrolidin-1-yl-3a,4,5,9b-tetrahydro-naphtho[1,2-d][1,2,3]triazol-3-yl)-phosphonic acid di-p-tolyl ester

1,3-diphenyl-4,5-dihydro-3H-benzo[e]indazole