Technology Process of 2-Cyclohexen-1-one,
4-(2,5-dimethoxyphenyl)-4-methyl-3-[1-(trimethylsilyl)ethenyl]-
There total 7 articles about 2-Cyclohexen-1-one,
4-(2,5-dimethoxyphenyl)-4-methyl-3-[1-(trimethylsilyl)ethenyl]- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
cerium(III) chloride;
In
tetrahydrofuran; diethyl ether;
for 14h;
Ambient temperature;
DOI:10.1021/jo970570q
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 63 percent / Jones reagent / acetone / 1 h / 0 °C
2: 84 percent / NaH / tetrahydrofuran / 1.) 0 deg C to room temperature, 30 min, 2.) 0 deg C, 1 h; room temperature, 4 h
3: 626 mg / t-BuOK / tetrahydrofuran / 1.) 30 min, 2.) 3 d
4: 91 percent / p-TsOH / 2 h / Heating
5: 64 percent / cerium chloride / diethyl ether; tetrahydrofuran / 14 h / Ambient temperature
With
jones reagent; cerium(III) chloride; potassium tert-butylate; sodium hydride; toluene-4-sulfonic acid;
In
tetrahydrofuran; diethyl ether; acetone;
DOI:10.1021/jo970570q
- Guidance literature:
-
Multi-step reaction with 2 steps
1: t-BuLi / diethyl ether; pentane / 2.5 h / -78 - -15 °C
2: 64 percent / cerium chloride / diethyl ether; tetrahydrofuran / 14 h / Ambient temperature
With
cerium(III) chloride; tert.-butyl lithium;
In
tetrahydrofuran; diethyl ether; pentane;
DOI:10.1021/jo970570q
