Technology Process of CID 110916
There total 8 articles about CID 110916 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
peracetic acid; sodium carbonate;
In
dichloromethane; acetic acid;
at 0 - 20 ℃;
for 3h;
Inert atmosphere;
DOI:10.1021/ol802104z
- Guidance literature:
-
With
3-chloro-benzenecarboperoxoic acid;
In
chloroform;
at 20 ℃;
for 17h;
DOI:10.1002/anie.201309847
- Guidance literature:
-
With
3-chloro-benzenecarboperoxoic acid;
In
dichloromethane;
other reagents: H2O2/KHCO3/dicyclohexylcarbodiimide, H2O2/Na3PO4*12H2O/dicyclohexylcarbodiimide, H2O2/Amberlite IRC-50/dicyclohexylcarbodiimide, H2O2/KHCO3/benzonitrile;
DOI:10.1021/jo972026n
