Oxiraneethanol, 3-phenyl-, (2R,3R)-rel-

Base Information

Chemical Name:Oxiraneethanol, 3-phenyl-, (2R,3R)-rel-
CAS No.:199534-08-2
Molecular Formula:C10H12O2
Molecular Weight:164.204
Hs Code.:

Synonyms:

Suppliers and Price of Oxiraneethanol, 3-phenyl-, (2R,3R)-rel-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Oxiraneethanol, 3-phenyl-, (2R,3R)-rel-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Oxiraneethanol, 3-phenyl-, (2R,3R)-rel-

There total 4 articles about Oxiraneethanol, 3-phenyl-, (2R,3R)-rel- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 937-58-6,20047-19-2,770-36-5
(3E)-4-phenyl-3-buten-1-ol

: 199534-08-2
4-phenyl-3,4-epoxy-1-butanol

Guidance literature:: With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 - 20 ℃;
DOI:10.1016/j.tet.2009.02.013

Reference yield:

: 770-36-5,20047-19-2,937-58-6
4-phenylbuta-3-en-1-ol

: 199534-08-2
4-phenyl-3,4-epoxy-1-butanol

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; water; at 0 ℃; for 1.5h; Inert atmosphere;
DOI:10.1002/chem.202004455

Reference yield:

: 122-78-1
phenylacetaldehyde

: 199534-08-2
4-phenyl-3,4-epoxy-1-butanol

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid; piperidine / dimethyl sulfoxide / 16.5 h / 100 °C / Inert atmosphere

2.1: lithium aluminium tetrahydride / diethyl ether / 2 h / 0 - 20 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

3.1: 3-chloro-benzenecarboperoxoic acid / water; dichloromethane / 1.5 h / 0 °C / Inert atmosphere

With piperidine; lithium aluminium tetrahydride; acetic acid; 3-chloro-benzenecarboperoxoic acid; In diethyl ether; dichloromethane; water; dimethyl sulfoxide;
DOI:10.1002/chem.202004455