3-Vinylbenzoyl chloride

Base Information

Chemical Name:3-Vinylbenzoyl chloride
CAS No.:20161-52-8
Molecular Formula:C9H7ClO
Molecular Weight:166.607
Hs Code.:2916399090
DSSTox Substance ID:DTXSID60501866
Mol file:20161-52-8.mol

Synonyms:3-Vinylbenzoyl chloride;3-vinylbenzoic acid chloride;20161-52-8;3-Ethenylbenzoyl chloride;SCHEMBL2941744;DTXSID60501866;ASAANMJKRKZQQI-UHFFFAOYSA-N

Suppliers and Price of 3-Vinylbenzoyl chloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 3-Vinylbenzoyl chloride

Chemical Property:

Boiling Point:247.4±19.0 °C(Predicted)
PSA：17.07000
Density:1.174±0.06 g/cm3(Predicted)
LogP:2.70860
XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:166.0185425
Heavy Atom Count:11
Complexity:165

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=CC1=CC(=CC=C1)C(=O)Cl

Technology Process of 3-Vinylbenzoyl chloride

There total 2 articles about 3-Vinylbenzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 28447-20-3
3-vinylbenzoic acid

: 20161-52-8
3-vinylbenzoyl chloride

Guidance literature:: With pyridine; thionyl chloride; In tetrahydrofuran; at 80 ℃; for 2h;
DOI:10.1021/jm990326m

Reference yield:

: 20161-52-8
3-vinylbenzoyl chloride

Guidance literature:: m-Vinylbenzoesaeure, SOCl2 (ohne Detaile);

Reference yield: 76.0%

: 20161-52-8
3-vinylbenzoyl chloride

: 115437-18-8
7-triethylsilyl-10-deacetylbaccatin III

: (2aR,4S,4aS,6R,9S,11S,12S,12aR,12bS)-12b-acetoxy-12-(benzoyloxy)-9,11-dihydroxy-4a,8,13,13-tetramethyl-5-oxo-4-((triethylsilyl)oxy)-2a,3,4,4a,5,6,9,10,11,12,12a,12b-dodecahydro-1H-7,11-methanocyclodeca[3,4]benzo[1,2-b]oxet-6-yl 3-vinylbenzoate

Guidance literature:: 7-triethylsilyl-10-deacetylbaccatin III; With lithium hexamethyldisilazane; In tetrahydrofuran; at -40 ℃; for 0.5h; Inert atmosphere;

3-vinylbenzoyl chloride; In tetrahydrofuran; at -40 ℃; for 0.5h; Inert atmosphere;
DOI:10.1002/anie.201901874