1,1-Diphenylgermetane

Base Information

Chemical Name:1,1-Diphenylgermetane
CAS No.:202208-97-7
Molecular Formula:C15H16Ge
Molecular Weight:268.882
Hs Code.:
DSSTox Substance ID:DTXSID20571868
Nikkaji Number:J948.214H
Wikidata:Q82460052

Synonyms:1,1-Diphenylgermetane;202208-97-7;DTXSID20571868

Suppliers and Price of 1,1-Diphenylgermetane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 0 raw suppliers

Chemical Property of 1,1-Diphenylgermetane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:2
Exact Mass:270.0463783
Heavy Atom Count:16
Complexity:200

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C[Ge](C1)(C2=CC=CC=C2)C3=CC=CC=C3

Technology Process of 1,1-Diphenylgermetane

There total 1 articles about 1,1-Diphenylgermetane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 109-64-8
1,3-dibromo-propane

: 1613-66-7
dichlorodiphenylgermane

: 202208-97-7
1,1-diphenylgermacyclobutane

Guidance literature:: With magnesium; In diethyl ether; stirring (over night, room temp.), rapidly addn. of germanium-complex, stirring (8 h), decantation (ice bath), quenching (NH4Cl); organic layer sepn., washing (water, sodium bicarbonate, water), drying (MgSO4), solvent removing (evapn.), chromy. work up (silica, hexane); elem. anal.;
DOI:10.1021/ja973756f

Reference yield:

: 202208-97-7
1,1-diphenylgermacyclobutane

: 202208-99-9
1,1,3,3-tetraphenyl-1,3-digermacyclobutane

Guidance literature:: In hexane; byproducts: C2H4; Irradiation (UV/VIS); irradiation (8 h); solvent removing (evapn.), chromy. work up (hexane, dichlormethane in hexane), crystn. (add. pentane, -10°C), recrystn. (pentane); elem. anal.;
DOI:10.1021/ja973756f