Technology Process of Decanoic acid, 2-chloro-, methyl ester
There total 1 articles about Decanoic acid, 2-chloro-, methyl ester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
chlorine;
at 20 ℃;
Product distribution;
Irradiation;
other temperature; also with SO2Cl2 (60 deg C, Bz2O2, dark);
- Guidance literature:
-
2-chloro-decanoic acid methyl ester;
With
potassium carbonate;
In
tetrahydrofuran;
at 60 ℃;
for 4h;
Inert atmosphere;
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium carbonate / tetrahydrofuran / 4 h / 60 °C / Inert atmosphere
1.2: Inert atmosphere
2.1: phosphorus tribromide / 1,2-dichloro-ethane / 3 h / 60 °C / Inert atmosphere
3.1: magnesium / tetrahydrofuran / 3 h / 50 °C / Inert atmosphere
4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / 20 °C / Inert atmosphere
5.1: 4-acetylamino-2,2,6,6-tetramethyl-1-piperidinoxy / 1,2-dichloro-ethane / 4 h / 40 °C / Inert atmosphere
With
4-acetylamino-2,2,6,6-tetramethyl-1-piperidinoxy; phosphorus tribromide; potassium carbonate; magnesium; 3-chloro-benzenecarboperoxoic acid;
In
tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane;