Dibenzyl cyclohexane-1,1-dicarboxylate

Base Information

Chemical Name:Dibenzyl cyclohexane-1,1-dicarboxylate
CAS No.:208662-21-9
Molecular Formula:C22H24O4
Molecular Weight:352.43
Hs Code.:
DSSTox Substance ID:DTXSID00572570
Nikkaji Number:J954.896C
Wikidata:Q82460957

Synonyms:Dibenzyl cyclohexane-1,1-dicarboxylate;208662-21-9;SCHEMBL7228727;DTXSID00572570;HKBXIFBGZWONDJ-UHFFFAOYSA-N

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Dibenzyl cyclohexane-1,1-dicarboxylate

Chemical Property:

XLogP3:5.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:8
Exact Mass:352.16745924
Heavy Atom Count:26
Complexity:419

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC(CC1)(C(=O)OCC2=CC=CC=C2)C(=O)OCC3=CC=CC=C3

Technology Process of Dibenzyl cyclohexane-1,1-dicarboxylate

There total 4 articles about Dibenzyl cyclohexane-1,1-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

: 2-(2-Iodo-ethyl)-2-(3-oxo-propyl)-malonic acid dibenzyl ester

: 208662-21-9
dibenzyl cyclohexane-1,1-dicarboxylate

: 4-Hydroxy-cyclohexane-1,1-dicarboxylic acid dibenzyl ester

Guidance literature:: With tri-n-butyl-tin hydride; triphenylphosphine; In benzene; for 3h; Ambient temperature; Irradiation;
DOI:10.1055/s-1998-1712

Reference yield:

: 15014-25-2
malonic acid dibenzyl ester

: 208662-21-9
dibenzyl cyclohexane-1,1-dicarboxylate

Guidance literature:: With potassium carbonate; In dimethyl sulfoxide;
DOI:10.1021/ol034707c

Reference yield:

: 2-allyl-2-(but-3-en-1-yl)malonate

: 208662-21-9
dibenzyl cyclohexane-1,1-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: Hoveyda-Grubbs catalyst second generation / 1,2-dichloro-ethane / 0.5 h / Inert atmosphere

2: sodium tetrahydroborate / methanol / 3 h / Inert atmosphere

With sodium tetrahydroborate; Hoveyda-Grubbs catalyst second generation; In methanol; 1,2-dichloro-ethane;
DOI:10.1021/ol5019739