1H-Indole-2-carboxylic acid, 5-methoxy-, hydrazide

Base Information

• Chemical Name: 1H-Indole-2-carboxylic acid, 5-methoxy-, hydrazide
• CAS No.: 20948-65-6
• Molecular Formula: C10H11N3O2
• Molecular Weight: 205.216
• Hs Code.: 2933990090
• Mol file: 20948-65-6.mol

Synonyms:2,3-DIHYDRO-5-METHOXY-1H-INDENE-4-CARBOXALDEHYDE;5-methoxy-indole-2-carboxylic acid hydrazide;5-methoxy-indan-4-carbaldehyde;

Chemical Property of 1H-Indole-2-carboxylic acid, 5-methoxy-, hydrazide

Chemical Property:

• PSA: 80.14000
• LogP: 1.87120

Purity/Quality:

98%min ^*data from raw suppliers

5-Methoxy-1H-indole-2-carboxylicAcidHydrazide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1H-Indole-2-carboxylic acid, 5-methoxy-, hydrazide

There total 4 articles about 1H-Indole-2-carboxylic acid, 5-methoxy-, hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

methyl 5-methoxyindole-2-carboxylate (67929-86-6) → 5-methoxy-1H-Indole-2-carbohydrazide (20948-65-6)

Guidance literature:

With hydrazine hydrate; In methanol; Reflux;

DOI:10.3390/molecules22111958

Reference yield: 80.0%

ethyl 5-methoxy-1H-indole-2-carboxylate (4792-58-9) → 5-methoxy-1H-Indole-2-carbohydrazide (20948-65-6)

Guidance literature:

With hydrazine; In ethanol; for 96h; Reflux;

DOI:10.1007/s11030-021-10253-z

Reference yield:

5-methoxy-1H-indole-2-carboxylic acid (4382-54-1) → 5-methoxy-1H-Indole-2-carbohydrazide (20948-65-6)

Guidance literature:

Multi-step reaction with 2 steps

1: sulfuric acid / 4 h / Reflux

2: hydrazine hydrate / methanol / Reflux

With hydrazine hydrate; sulfuric acid; In methanol;

DOI:10.3390/molecules22111958

upstream raw materials:

ethyl 5-methoxy-1H-indole-2-carboxylate

5-methoxy-1H-indole-2-carboxylic acid

methyl 5-methoxyindole-2-carboxylate

Downstream raw materials:

1-phenyl-3-(5'-methoxy-indole-2'-carboxamido)-thiourea

C₁₆H₁₅N₃O₄S

5-methoxy-2-(5'-mercapto-4'-phenyl-1',2',4'-triazol-3'-yl)indole

5-methoxy-2-(5'-phenylamino-1',3',4'-oxadiazol-2'-yl)indole

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