p-(n-Dodecyl)benzoicacid

Base Information

• Chemical Name: p-(n-Dodecyl)benzoicacid
• CAS No.: 21021-55-6
• Molecular Formula: C19H30O2
• Molecular Weight: 290.446
• Hs Code.: 2916399090
• Mol file: 21021-55-6.mol

Synonyms:Benzoic acid,4-dodecyl;4-Dodecyl-benzoesaeure;4-dodecyl-benzoic acid;4-n-Dodecylbenzoic acid;

Chemical Property of p-(n-Dodecyl)benzoicacid

Chemical Property:

• PSA: 37.30000
• LogP: 5.84820

Purity/Quality:

98%Min ^*data from raw suppliers

4-N-DODECYLBENZOIC ACID 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of p-(n-Dodecyl)benzoicacid

There total 13 articles about p-(n-Dodecyl)benzoicacid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

4-dodecylbenzaldehyde (110675-86-0) → 4-dodecylbenzoic acid (21021-55-6)

Guidance literature:

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; In tetrahydrofuran; water; tert-butyl alcohol; at 20 ℃; for 1h;

Reference yield: 63.0%

4-n-dodecylbenzoyl chloride (53097-40-8) → 4-dodecylbenzoic acid (21021-55-6)

Guidance literature:

With sodium hydroxide; In water;

DOI:10.1021/jo00197a012

Reference yield:

1-dodecylbenzene (123-01-3) → 4-dodecylbenzoic acid (21021-55-6)

Guidance literature:

Multi-step reaction with 2 steps

1: AlCl₃ / CH₂Cl₂

2: 63 percent / NaOH / H₂O

With sodium hydroxide; aluminium trichloride; In dichloromethane; water;

DOI:10.1021/jo00197a012

upstream raw materials:

4-dodecylacetophenone

(E)-4-(4-n-dodecylphenyl)-4-oxo-2-butenoic acid

4-n-dodecylbenzoyl chloride

bromoundecane

Downstream raw materials:

4-Dodecyl-2-iodo-benzoic acid

1,3-Dicyclohexylurea

1-tert-Butoxymethyl-4-dodecyl-benzene

7-(tert-butyldimethylsilyloxy)-8-methylnaphthalen-2-yl 4-(4-dodecylbenzoyloxy)benzoate