4-dodecylbenzaldehyde

Base Information

• Chemical Name: 4-dodecylbenzaldehyde
• CAS No.: 110675-86-0
• Molecular Formula: C₁₉H₃₀O
• Molecular Weight: 274.447
• Mol file: 110675-86-0.mol

Synonyms:4-dodecylbenzaldehyde

Chemical Property of 4-dodecylbenzaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-dodecylbenzaldehyde

There total 9 articles about 4-dodecylbenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

1-dodecene (112-41-4,25067-08-7,62132-67-6) + 4-bromo-benzaldehyde (1122-91-4) → 4-dodecylbenzaldehyde (110675-86-0)

Guidance literature:

1-dodecene; With 9-borabicyclo[3.3.1]nonane; In tetrahydrofuran;

4-bromo-benzaldehyde; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium hydroxide; In tetrahydrofuran; for 4h; Reflux;

Reference yield: 70.0%

1-bromo-4-dodecylbenzene (126930-72-1) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → 4-dodecylbenzaldehyde (110675-86-0)

Guidance literature:

1-bromo-4-dodecylbenzene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

N,N-dimethyl-formamide;

DOI:10.1142/S1088424612500629

Reference yield: 70.0%

1-dodecylbenzene (123-01-3) + hexamethylenetetramine (100-97-0) → 4-dodecylbenzaldehyde (110675-86-0)

Guidance literature:

With trifluoroacetic acid; at 80 ℃; Heating;

DOI:10.1021/jp962001c

upstream raw materials:

trimethylamine-N-oxide

4-dodecylbenzyl chloride

1-dodecylbenzene

Ethyl oxalyl chloride

Downstream raw materials:

hexa(pyrrol-yl)hexaazatrinaphthalene

2-(4-dodecylbenzoyl)hydrazinecarboximidamide hydrochloride

tert-butyl (((tert-butoxycarbonyl)imino)(2-(4-dodecylbenzoyl)hydrazinyl)methyl)carbamate

methyl 4-n-dodecylbenzoate