2,4-Heptadienal, 6,6-dimethyl-2,4-bis(phenylthio)-, (2Z,4Z)-

Base Information

Chemical Name:2,4-Heptadienal, 6,6-dimethyl-2,4-bis(phenylthio)-, (2Z,4Z)-
CAS No.:210416-91-4
Molecular Formula:C21H22OS2
Molecular Weight:354.537
Hs Code.:

Synonyms:

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Chemical Property of 2,4-Heptadienal, 6,6-dimethyl-2,4-bis(phenylthio)-, (2Z,4Z)-

Chemical Property:

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Technology Process of 2,4-Heptadienal, 6,6-dimethyl-2,4-bis(phenylthio)-, (2Z,4Z)-

There total 7 articles about 2,4-Heptadienal, 6,6-dimethyl-2,4-bis(phenylthio)-, (2Z,4Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 210416-90-3
(1Z,4Z)-1-Ethoxy-6,6-dimethyl-2,4-bis-phenylsulfanyl-hepta-1,4-dien-3-ol

: 210416-91-4
6,6-dimethyl-2,4-bis(phenylthio)hepta-2,4-dienal

Guidance literature:: With polyphosphoric acid trimethylsilyl ester; In 1,2-dichloro-ethane;
DOI:10.1021/jo980487i

Reference yield:

: 630-19-3
pivalaldehyde

: 210416-91-4
6,6-dimethyl-2,4-bis(phenylthio)hepta-2,4-dienal

Guidance literature:: Multi-step reaction with 4 steps

1: 81 percent / BuLi / tetrahydrofuran / -70 °C

2: 88 percent / polyphosphoric acid trimethyl ester / 1,2-dichloro-ethane / 83 °C

3: n-BuLi / -70 °C

4: 62 percent / polyphosphoric acid trimethylsilyl ester / 1,2-dichloro-ethane

With n-butyllithium; polyphosphoric acid trimethylsilyl ester; polyphosphoric acid trimethyl ester; In tetrahydrofuran; 1,2-dichloro-ethane;
DOI:10.1021/jo980487i

Reference yield:

: 210416-70-9
(Z)-1-Ethoxy-4,4-dimethyl-2-phenylsulfanyl-pent-1-en-3-ol

: 210416-91-4
6,6-dimethyl-2,4-bis(phenylthio)hepta-2,4-dienal

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / polyphosphoric acid trimethyl ester / 1,2-dichloro-ethane / 83 °C

2: n-BuLi / -70 °C

3: 62 percent / polyphosphoric acid trimethylsilyl ester / 1,2-dichloro-ethane

With n-butyllithium; polyphosphoric acid trimethylsilyl ester; polyphosphoric acid trimethyl ester; In 1,2-dichloro-ethane;
DOI:10.1021/jo980487i