N-methyl-N-(1-phenylethyl)-2-propynylamine

Base Information

• Chemical Name: N-methyl-N-(1-phenylethyl)-2-propynylamine
• CAS No.: 2322-04-5
• Molecular Formula: C12H15 N
• Molecular Weight: 0
• Hs Code.: 2921499090
• Mol file: 2322-04-5.mol

Synonyms:Benzenemethanamine,N,a-dimethyl-N-2-propynyl- (9CI);Benzylamine, N,a-dimethyl-N-2-propynyl-(7CI,8CI)

Chemical Property of N-methyl-N-(1-phenylethyl)-2-propynylamine

Chemical Property:

• Vapor Pressure: 0.0473mmHg at 25°C
• Boiling Point: 236.5°C at 760 mmHg
• Flash Point: 88.3°C
• PSA: 3.24000
• Density: 0.962g/cm³
• LogP: 2.31260

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-methyl-N-(1-phenylethyl)-2-propynylamine

There total 2 articles about N-methyl-N-(1-phenylethyl)-2-propynylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

N-methyl-N-(1-phenylethyl)amine (42882-26-8) + propargyl bromide (106-96-7) → N,α-dimethyl-N-2-propynylbenzenemethanamine (2322-04-5)

Guidance literature:

With tetrabutylammomium bromide; potassium carbonate; In water; toluene; for 24h; Ambient temperature;

Reference yield: 75.0%

phenylmagnesium bromide + acetaldehyde (75-07-0,9002-91-9) + propargyl bromide (106-96-7) + methyl trifluoromethanesulfonate (333-27-7) → N,α-dimethyl-N-2-propynylbenzenemethanamine (2322-04-5)

Guidance literature:

Multistep reaction;

DOI:10.1016/S0040-4039(00)01104-7

upstream raw materials:

N-methyl-N-(1-phenylethyl)amine

propargyl bromide

acetaldehyde

methyl trifluoromethanesulfonate

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