Tert-butyl N-[2-(4-bromophenyl)propyl]carbamate

Base Information

Chemical Name:Tert-butyl N-[2-(4-bromophenyl)propyl]carbamate
CAS No.:211314-91-9
Molecular Formula:C14H20BrNO2
Molecular Weight:314.222
Hs Code.:
DSSTox Substance ID:DTXSID801211096
Mol file:211314-91-9.mol

Synonyms:211314-91-9;tert-Butyl 2-(4-bromophenyl)propylcarbamate;Tert-butyl N-[2-(4-bromophenyl)propyl]carbamate;Carbamic acid, N-[2-(4-bromophenyl)propyl]-, 1,1-dimethylethyl ester;SCHEMBL255676;DWVQIDLQGUKRLS-UHFFFAOYSA-N;DTXSID801211096;A50843;tert-Butyl (2-(4-bromophenyl)propyl)carbamate;EN300-12457674;1,1-Dimethylethyl N-[2-(4-bromophenyl)propyl]carbamate;[2-(4-Bromo-phenyl)-propyl]-carbamic acid tert-butyl ester

Suppliers and Price of Tert-butyl N-[2-(4-bromophenyl)propyl]carbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Tert-butyl N-[2-(4-bromophenyl)propyl]carbamate

Chemical Property:

XLogP3:3.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:5
Exact Mass:313.06774
Heavy Atom Count:18
Complexity:268

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(CNC(=O)OC(C)(C)C)C1=CC=C(C=C1)Br

Technology Process of Tert-butyl N-[2-(4-bromophenyl)propyl]carbamate

There total 5 articles about Tert-butyl N-[2-(4-bromophenyl)propyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 256381-13-2
2-(4-bromophenyl)propan-1-amine

: 211314-91-9
1-[(1-tert-butoxycarbonylamino-1-methyl)ethyl]-4-bromobenzene

Guidance literature:: With sodium hydrogencarbonate; In chloroform; at 20 ℃; for 1h;
DOI:10.1021/jm0002836

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 211314-90-8
2-(4-Bromophenyl)propylamine hydrochloride

: 211314-91-9
1-[(1-tert-butoxycarbonylamino-1-methyl)ethyl]-4-bromobenzene

Guidance literature:: With sodium hydrogencarbonate; In chloroform;

Reference yield:

: 16532-79-9
4-Bromophenylacetonitrile

: 211314-91-9
1-[(1-tert-butoxycarbonylamino-1-methyl)ethyl]-4-bromobenzene

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / 16 h / 180 °C

2: BH₃*SMe₂ / tetrahydrofuran / Heating

3: satd. NaHCO₃ / CHCl₃ / 1 h / 20 °C

With dimethylsulfide borane complex; sodium hydrogencarbonate; potassium carbonate; In tetrahydrofuran; chloroform;
DOI:10.1021/jm0002836