(1E)-N-hydroxy-2-(morpholin-4-yl)-1-phenylethanimine

Base Information

• Chemical Name: (1E)-N-hydroxy-2-(morpholin-4-yl)-1-phenylethanimine
• CAS No.: 15437-09-9
• Molecular Formula: C12H16 N2 O2
• Molecular Weight: 220.2676
• NSC Number: 304612,150246
• Nikkaji Number: J469.483J

Synonyms:NSC150246;UBAXQEDBBHSFET-SEYXRHQNSA-;UBAXQEDBBHSFET-SEYXRHQNSA-N;HMS1443P21;NSC304612;STK694122;(Z)-alpha-Morpholinoacetophenone oxime;AKOS005605251;NSC-150246;NSC-304612;IDI1_015962;15437-09-9;(1E)-N-hydroxy-2-(morpholin-4-yl)-1-phenylethanimine;InChI=1/C12H16N2O2/c15-13-12(11-4-2-1-3-5-11)10-14-6-8-16-9-7-14/h1-5,15H,6-10H2/b13-12-

Chemical Property of (1E)-N-hydroxy-2-(morpholin-4-yl)-1-phenylethanimine

Chemical Property:

• Vapor Pressure: 5.22E-06mmHg at 25°C
• Boiling Point: 366.3°Cat760mmHg
• Flash Point: 175.3°C
• Density: 1.17g/cm³
• XLogP3: 1.6
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 3
• Exact Mass: 220.121177757
• Heavy Atom Count: 16
• Complexity: 231

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1COCCN1CC(=NO)C2=CC=CC=C2
• Isomeric SMILES: C1COCCN1C/C(=N/O)/C2=CC=CC=C2

Technology Process of (1E)-N-hydroxy-2-(morpholin-4-yl)-1-phenylethanimine

There total 2 articles about (1E)-N-hydroxy-2-(morpholin-4-yl)-1-phenylethanimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

morpholine (110-91-8,99108-56-2) + (Z)-2-chloro-1-phenylethan-1-one oxime (40814-66-2) → anti-Morpholinoacetophenone oxime (15437-08-8,91557-33-4) + syn-α-Morpholinoacetophenone oxime (15437-09-9,91557-33-4)

Guidance literature:

In methanol; Product distribution; other solvent;

DOI:10.1016/S0040-4020(01)86809-5

Reference yield:

→ syn-α-Morpholinoacetophenone oxime (15437-09-9,91557-33-4)

Guidance literature:

ω-Morpholino-acetophenon, H2N-OH*HCl, aq. NaOH, EtOH;

Reference yield:

syn-α-Morpholinoacetophenone oxime (15437-09-9,91557-33-4) → 2-(morpholin-4-yl)-1-phenylethan-1-amine (38060-08-1)

Guidance literature:

With ethanol; sodium;

DOI:10.1021/ja01234a006

upstream raw materials:

morpholine

(Z)-2-chloro-1-phenylethan-1-one oxime

Downstream raw materials:

2-(morpholin-4-yl)-1-phenylethan-1-amine

2-morpholin-4-yl-1-phenyl-ethanone O-(1-methoxy-1-methyl-ethyl)-oxime

2-phenyl-5,6,8,8a-tetrahydro-3H-imidazo[2,1-c][1,4]oxazine 1-oxide

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