6-FORMYL-PYRIDINE-2-CARBOXYLIC ACID ETHYL ESTER

Base Information

• Chemical Name: 6-FORMYL-PYRIDINE-2-CARBOXYLIC ACID ETHYL ESTER
• CAS No.: 21908-10-1
• Molecular Formula: C9H9NO3
• Molecular Weight: 179.17300
• Hs Code.: 2933399090
• Mol file: 21908-10-1.mol

Synonyms:6-Formyl-pyridine-2-carboxylic acid ethyl ester;6-formyl-2-picolinic acid ethyl ester;ethyl 6-formyl-2-pyridinecarboxylate;Ethyl 6-formylpicolinate;2-Formyl-pyridin-carbonsaeure-(6)-ethylester;

Chemical Property of 6-FORMYL-PYRIDINE-2-CARBOXYLIC ACID ETHYL ESTER

Chemical Property:

• PSA: 56.26000
• LogP: 1.07080
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

Ethyl6-Formylpyridine-2-carboxylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6-FORMYL-PYRIDINE-2-CARBOXYLIC ACID ETHYL ESTER

There total 5 articles about 6-FORMYL-PYRIDINE-2-CARBOXYLIC ACID ETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

ethyl 6-(dibromomethyl)pyridine-2-carboxylate → ethyl 6-formyl-2-pyridinecarboxylate (21908-10-1)

Guidance literature:

ethyl 6-(dibromomethyl)pyridine-2-carboxylate; With pyridine; at 100 ℃; for 1.33333h;

With water; Further stages.;

DOI:10.1016/j.tet.2007.11.030

Reference yield:

ethyl 6-methylpyridine-2-carboxylate (39640-51-2) → ethyl 6-formyl-2-pyridinecarboxylate (21908-10-1)

Guidance literature:

ethyl 6-methylpyridine-2-carboxylate; With selenium(IV) oxide; acetic acid; for 48h; Heating / reflux;

With sodium hydrogencarbonate; In water; pH=6;

Reference yield:

ethyl 6-(hydroxymethyl)pyridine-2-carboxylate (41337-81-9) → ethyl 6-formyl-2-pyridinecarboxylate (21908-10-1)

Guidance literature:

With sulfur trioxide pyridine complex; dimethyl sulfoxide; triethylamine; In dichloromethane; at 4 - 20 ℃;

DOI:10.1021/op100072y

upstream raw materials:

ethyl 6-methylpyridine-2-carboxylate

diethyl-2,6-pyridinedicarbonyl ester

ethyl 6-(hydroxymethyl)pyridine-2-carboxylate

Downstream raw materials:

C₁₈H₁₉NO₆

C₁₅H₁₄N₂O₆

C₁₅H₁₄ClNO₄

ethyl 6-[(5-chloro-2-hydroxyphenyl)hydroxymethyl]-2-pyridinecarboxylate

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