2,3,10-trimethoxy-5,8,13,13a-tetrahydro-6H-isoquino[3,2-a]isoquinolin-11-amine

Base Information

Chemical Name:2,3,10-trimethoxy-5,8,13,13a-tetrahydro-6H-isoquino[3,2-a]isoquinolin-11-amine
CAS No.:50506-25-7
Molecular Formula:C₂₀H₂₄N₂O₃
Molecular Weight:340.422
Hs Code.:

Synonyms:11-Amino-2,3,10-trimethoxyberbine;11-Amino-5,6,13,13a-tetrahydro-2,3,10-trimethoxy-8H-dibenzo[a,g]quinolizine

Suppliers and Price of 2,3,10-trimethoxy-5,8,13,13a-tetrahydro-6H-isoquino[3,2-a]isoquinolin-11-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3,10-trimethoxy-5,8,13,13a-tetrahydro-6H-isoquino[3,2-a]isoquinolin-11-amine

Chemical Property:

Vapor Pressure:5.33E-10mmHg at 25°C
Boiling Point:496.6°Cat760mmHg
Flash Point:254.1°C
Density:1.26g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,3,10-trimethoxy-5,8,13,13a-tetrahydro-6H-isoquino[3,2-a]isoquinolin-11-amine

There total 4 articles about 2,3,10-trimethoxy-5,8,13,13a-tetrahydro-6H-isoquino[3,2-a]isoquinolin-11-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 129011-60-5
1-(3-amino-4-methoxybenzyl)-1,2,3,4-tetrahydro-6,7-dimethoxyisoquinoline

: 50506-25-7
11-amino-5,6,13,13a-tetrahydro-2,3,10-trimethoxy-8H-dibenzoquinolizine

Guidance literature:: In ethanol; for 1h; Heating;

Reference yield:

: 75265-97-3
1,2,3,4-tetrahydro-6,7-dimethoxy-1-(4-methoxy-3-nitrobenzyl)isoquinoline

: 50506-25-7
11-amino-5,6,13,13a-tetrahydro-2,3,10-trimethoxy-8H-dibenzoquinolizine

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / SnCl₂*2H₂O, conc. HCl / acetic acid / 1 h

2: 75 percent / ethanol / 1 h / Heating

With hydrogenchloride; tin(ll) chloride; In ethanol; acetic acid;

Reference yield:

: 26870-64-4
N-(3,4-dimethoxyphenethyl)-2-(4-methoxy-3-nitrophenyl)acetamide

: 50506-25-7
11-amino-5,6,13,13a-tetrahydro-2,3,10-trimethoxy-8H-dibenzoquinolizine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) PCl₅, 2.) NaBH₃CN, MeOH / 1.) CHCl₃, RT, 6 h, 2.) THF, RT, 45 min

2: 72 percent / SnCl₂*2H₂O, conc. HCl / acetic acid / 1 h

3: 75 percent / ethanol / 1 h / Heating

With hydrogenchloride; methanol; phosphorus pentachloride; sodium cyanoborohydride; tin(ll) chloride; In ethanol; acetic acid;