N-(2-Formyl-4,5-dimethoxy-phenyl)-acetamide

Base Information

• Chemical Name: N-(2-Formyl-4,5-dimethoxy-phenyl)-acetamide
• CAS No.: 22608-86-2
• Molecular Formula: C11H13NO4
• Molecular Weight: 223.229
• Hs Code.: 2924299090
• DSSTox Substance ID: DTXSID20396119
• Wikidata: Q82196651
• Mol file: 22608-86-2.mol

Synonyms:N-(2-Formyl-4,5-dimethoxy-phenyl)-acetamide;N-(2-formyl-4,5-dimethoxyphenyl)acetamide;22608-86-2;SCHEMBL2890278;DTXSID20396119;N-(2-formyl-4,5-dimethoxy-phenyl)-acetamide, AldrichCPR

Chemical Property of N-(2-Formyl-4,5-dimethoxy-phenyl)-acetamide

Chemical Property:

• PSA: 68.12000
• LogP: 2.12420
• XLogP3: 1.1
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 4
• Exact Mass: 223.08445790
• Heavy Atom Count: 16
• Complexity: 256

Purity/Quality:

99% ^*data from raw suppliers

N-(2-FORMYL-4,5-DIMETHOXY-PHENYL)-ACETAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 36
• Safety Statements: 26

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=O)NC1=CC(=C(C=C1C=O)OC)OC

Technology Process of N-(2-Formyl-4,5-dimethoxy-phenyl)-acetamide

There total 9 articles about N-(2-Formyl-4,5-dimethoxy-phenyl)-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

acetic anhydride (108-24-7) + 2-amino-4,5-dimethoxybenzaldehyde (22608-87-3) → 2-acetylamino-4,5-dimethoxybenzaldehyde (22608-86-2)

Guidance literature:

With pyridine; at 55 - 60 ℃; for 0.25h;

DOI:10.1002/jhet.5570430315

Reference yield: 50.0%

N-(2-hydroxymethyl-4,5-dimethoxy-phenyl)-acetamide (1158910-11-2) → 2-acetylamino-4,5-dimethoxybenzaldehyde (22608-86-2)

Guidance literature:

With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 0.166667h;

Reference yield: 11.0%

N-(6,7-dimethoxy-2-methylquinazolin-3-io)-N-amide (74990-23-1) → O-Ethyl N-Butylthiocarbamate (55365-85-0) + 2-acetylamino-4,5-dimethoxybenzaldehyde (22608-86-2) + 2-amino-4,5-dimethoxybenzaldehyde (22608-87-3) + 2-amino-4,5-dimethoxybenzaldehyde hydrazone

Guidance literature:

In various solvent(s); for 3h; Ambient temperature; Irradiation;

upstream raw materials:

acetic anhydride

2-amino-4,5-dimethoxybenzaldehyde

N-(6,7-dimethoxy-2-methylquinazolin-3-io)-N-amide

acetyl chloride

Downstream raw materials:

(6,7-Dimethoxy-3-phenyl-quinolin-2-yl)-diethyl-amine

4-acetyl-5-(2-acetylamino-4,5-dimethoxyphenyl)-2-(3,4-dimethoxyphenyl)-Δ²-1,3,4-thiadiazoline

2-(3,4-Dimethoxy-phenyl)-7,8-dimethoxy-4-methyl-9bH-1-thia-3,3a,5-triaza-cyclopenta[a]naphthalene; compound with perchloric acid

2-(3,4-dimethoxyphenyl)-8,9-dimethoxy-5-methyl-10bH-<1,3,4>thiadiazolo<3,2-c>quinazoline

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