1,3-Cyclohexanedicarboxylic acid, monoethyl ester, (1S,3R)-

Base Information

Chemical Name:1,3-Cyclohexanedicarboxylic acid, monoethyl ester, (1S,3R)-
CAS No.:227783-03-1
Molecular Formula:C₁₀H₁₆O₄
Molecular Weight:200.235
Hs Code.:

Synonyms:1,3-Cyclohexanedicarboxylic acid,monoethyl ester,(1S,3R);

Suppliers and Price of 1,3-Cyclohexanedicarboxylic acid, monoethyl ester, (1S,3R)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 1,3-Cyclohexanedicarboxylic acid, monoethyl ester, (1S,3R)-

Chemical Property:

PSA：66.43000
LogP:0.10580

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,3-Cyclohexanedicarboxylic acid, monoethyl ester, (1S,3R)-

There total 1 articles about 1,3-Cyclohexanedicarboxylic acid, monoethyl ester, (1S,3R)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 62059-56-7
cis-1,3-Cyclohexanedicarboxylic acid diethyl ester

: 227783-03-1
(1S,3R)-Cyclohexane-1,3-dicarboxylic acid monoethyl ester

Guidance literature:: With pH 7 buffer; Pseudomonas cepacia PS-30 lipase; In water;
DOI:10.1016/S0957-4166(99)00060-9

Reference yield:

: 227783-03-1
(1S,3R)-Cyclohexane-1,3-dicarboxylic acid monoethyl ester

: 75-65-0
tert-butyl alcohol

: (1S,3R)-3-tert-Butoxycarbonylamino-cyclohexanecarboxylic acid ethyl ester

Guidance literature:: With diphenylphosphoranyl azide; triethylamine; In toluene; at 95 ℃;
DOI:10.1016/j.bmc.2005.01.033

Reference yield:

: 227783-03-1
(1S,3R)-Cyclohexane-1,3-dicarboxylic acid monoethyl ester

: 222530-34-9,218772-92-0,222530-33-8
(1S,3R)-3-((tert-butoxycarbonyl)amino)cyclo hexane-1-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: diphenylphosphoryl azide; triethylamine / toluene / 95 °C

2: aq. NaOH / tetrahydrofuran / 50 °C

With sodium hydroxide; diphenylphosphoranyl azide; triethylamine; In tetrahydrofuran; toluene; 1: Curtius rearrangement;
DOI:10.1016/j.bmc.2005.01.033