Carbonic acid, (1R,2S)-2-[[(1,1-dimethylethoxy)carbonyl]amino]-1-[[(2-methylpropyl)[(4- nitrophenyl)sulfonyl]amino]methyl]-3-phenylpropyl (3S)-tetrahydro-3-furanyl ester

Base Information

Chemical Name:Carbonic acid, (1R,2S)-2-[[(1,1-dimethylethoxy)carbonyl]amino]-1-[[(2-methylpropyl)[(4- nitrophenyl)sulfonyl]amino]methyl]-3-phenylpropyl (3S)-tetrahydro-3-furanyl ester
CAS No.:229495-71-0
Molecular Formula:C30H41N3O10S
Molecular Weight:635.736
Hs Code.:
Mol file:229495-71-0.mol

Carbonic acid,
(1R,2S)-2-[[(1,1-dimethylethoxy)carbonyl]amino]-1-[[(2-methylpropyl)[(4-
nitrophenyl)sulfonyl]amino]methyl]-3-phenylpropyl
(3S)-tetrahydro-3-furanyl ester

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Carbonic acid, (1R,2S)-2-[[(1,1-dimethylethoxy)carbonyl]amino]-1-[[(2-methylpropyl)[(4- nitrophenyl)sulfonyl]amino]methyl]-3-phenylpropyl (3S)-tetrahydro-3-furanyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Carbonic acid, (1R,2S)-2-[[(1,1-dimethylethoxy)carbonyl]amino]-1-[[(2-methylpropyl)[(4- nitrophenyl)sulfonyl]amino]methyl]-3-phenylpropyl (3S)-tetrahydro-3-furanyl ester

There total 2 articles about Carbonic acid, (1R,2S)-2-[[(1,1-dimethylethoxy)carbonyl]amino]-1-[[(2-methylpropyl)[(4- nitrophenyl)sulfonyl]amino]methyl]-3-phenylpropyl (3S)-tetrahydro-3-furanyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 86087-23-2,84921-89-1,864447-89-2
(S)-3-hydroxytetyrahydrofurane

: 229495-94-7
Carbonic acid (1R,2S)-2-tert-butoxycarbonylamino-1-{[isobutyl-(4-nitro-benzenesulfonyl)-amino]-methyl}-3-phenyl-propyl ester 4-nitro-phenyl ester

: 229495-71-0
Carbonic acid (1R,2S)-2-tert-butoxycarbonylamino-1-{[isobutyl-(4-nitro-benzenesulfonyl)-amino]-methyl}-3-phenyl-propyl ester (S)-(tetrahydro-furan-3-yl) ester

Guidance literature:: With triethylamine; In 1,4-dioxane; for 48h; Heating;
DOI:10.1016/S0960-894X(03)00463-3

Reference yield:

: 191226-98-9
[(1S,2R)-3-[(4-nitrophenylsulfonyl)(2-methylpropyl)amino]-2-hydroxy-1-(phenylmethyl)propyl]carbamic acid tert-butyl ester

: 229495-71-0
Carbonic acid (1R,2S)-2-tert-butoxycarbonylamino-1-{[isobutyl-(4-nitro-benzenesulfonyl)-amino]-methyl}-3-phenyl-propyl ester (S)-(tetrahydro-furan-3-yl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / LiOH*H₂O / dimethylformamide / 2 h / 20 °C

2: 100 percent / Et₃N / dioxane / 48 h / Heating

With lithium hydroxide; triethylamine; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(03)00463-3