Carbonic acid, (1R,2S)-2-[[(1,1-dimethylethoxy)carbonyl]amino]-1-[[(2-methylpropyl)[(4- nitrophenyl)sulfonyl]amino]methyl]-3-phenylpropyl 4-nitrophenyl ester

Base Information

Chemical Name:Carbonic acid, (1R,2S)-2-[[(1,1-dimethylethoxy)carbonyl]amino]-1-[[(2-methylpropyl)[(4- nitrophenyl)sulfonyl]amino]methyl]-3-phenylpropyl 4-nitrophenyl ester
CAS No.:229495-94-7
Molecular Formula:C32H38N4O11S
Molecular Weight:686.74
Hs Code.:

Carbonic acid,
(1R,2S)-2-[[(1,1-dimethylethoxy)carbonyl]amino]-1-[[(2-methylpropyl)[(4-
nitrophenyl)sulfonyl]amino]methyl]-3-phenylpropyl 4-nitrophenyl ester

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Carbonic acid, (1R,2S)-2-[[(1,1-dimethylethoxy)carbonyl]amino]-1-[[(2-methylpropyl)[(4- nitrophenyl)sulfonyl]amino]methyl]-3-phenylpropyl 4-nitrophenyl ester

Chemical Property:

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Technology Process of Carbonic acid, (1R,2S)-2-[[(1,1-dimethylethoxy)carbonyl]amino]-1-[[(2-methylpropyl)[(4- nitrophenyl)sulfonyl]amino]methyl]-3-phenylpropyl 4-nitrophenyl ester

There total 1 articles about Carbonic acid, (1R,2S)-2-[[(1,1-dimethylethoxy)carbonyl]amino]-1-[[(2-methylpropyl)[(4- nitrophenyl)sulfonyl]amino]methyl]-3-phenylpropyl 4-nitrophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 5070-13-3
bis-(p-nitrophenyl) carbonate

: 191226-98-9
[(1S,2R)-3-[(4-nitrophenylsulfonyl)(2-methylpropyl)amino]-2-hydroxy-1-(phenylmethyl)propyl]carbamic acid tert-butyl ester

: 229495-94-7
Carbonic acid (1R,2S)-2-tert-butoxycarbonylamino-1-{[isobutyl-(4-nitro-benzenesulfonyl)-amino]-methyl}-3-phenyl-propyl ester 4-nitro-phenyl ester

Guidance literature:: With lithium hydroxide; In N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1016/S0960-894X(03)00463-3

Reference yield: 100.0%

: 86087-23-2,84921-89-1,864447-89-2
(S)-3-hydroxytetyrahydrofurane

: 229495-94-7
Carbonic acid (1R,2S)-2-tert-butoxycarbonylamino-1-{[isobutyl-(4-nitro-benzenesulfonyl)-amino]-methyl}-3-phenyl-propyl ester 4-nitro-phenyl ester

: 229495-71-0
Carbonic acid (1R,2S)-2-tert-butoxycarbonylamino-1-{[isobutyl-(4-nitro-benzenesulfonyl)-amino]-methyl}-3-phenyl-propyl ester (S)-(tetrahydro-furan-3-yl) ester

Guidance literature:: With triethylamine; In 1,4-dioxane; for 48h; Heating;
DOI:10.1016/S0960-894X(03)00463-3

Reference yield:

: 229495-94-7
Carbonic acid (1R,2S)-2-tert-butoxycarbonylamino-1-{[isobutyl-(4-nitro-benzenesulfonyl)-amino]-methyl}-3-phenyl-propyl ester 4-nitro-phenyl ester

: Carbonic acid (1R,2S)-2-amino-1-{[isobutyl-(4-nitro-benzenesulfonyl)-amino]-methyl}-3-phenyl-propyl ester (S)-(tetrahydro-furan-3-yl) ester; compound with trifluoro-acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / Et₃N / dioxane / 48 h / Heating

2: CH₂Cl₂ / 0.5 h

With triethylamine; In 1,4-dioxane; dichloromethane;
DOI:10.1016/S0960-894X(03)00463-3