sodium alpha-hydroxy-3,4-methylenedioxytoluene-alpha-sulphonate

Base Information

• Chemical Name: sodium alpha-hydroxy-3,4-methylenedioxytoluene-alpha-sulphonate
• CAS No.: 37589-10-9
• Molecular Formula: C8H8 O6 S . Na
• Molecular Weight: 254.196
• Hs Code.: 2932999099
• Mol file: 37589-10-9.mol

Synonyms:1,3-Benzodioxole-5-methanesulfonicacid, a-hydroxy-, monosodium salt (9CI);Heloplex

Chemical Property of sodium alpha-hydroxy-3,4-methylenedioxytoluene-alpha-sulphonate

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 104.27000
• Density: g/cm³
• LogP: 1.03220

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of sodium alpha-hydroxy-3,4-methylenedioxytoluene-alpha-sulphonate

There total 1 articles about sodium alpha-hydroxy-3,4-methylenedioxytoluene-alpha-sulphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

piperonal (120-57-0,30024-74-9) → sodium benzo[d][1,3]dioxol-5-yl(hydroxy)methanesulfonate (37589-10-9)

Guidance literature:

With sodium hydrogensulfite; In ethanol; at 30 - 35 ℃; for 16h;

DOI:10.1016/j.tetlet.2014.03.046

Reference yield: 97.0%

5-(3-aminophenyl)-1H-tetrazole (73732-51-1) + sodium benzo[d][1,3]dioxol-5-yl(hydroxy)methanesulfonate (37589-10-9) → N-(benzo[d][1,3]dioxol-5-ylmethyl)-3-(1H-tetrazol-5-yl)aniline

Guidance literature:

With 2-picoline borane complex; acetic acid; In methanol; water; at 60 ℃; for 12h; Sealed tube; Inert atmosphere;

DOI:10.1021/acs.orglett.1c02604

Reference yield: 92.0%

sodium benzo[d][1,3]dioxol-5-yl(hydroxy)methanesulfonate (37589-10-9) → piperonal (120-57-0,30024-74-9)

Guidance literature:

With Montmorillonite KSF clay; for 0.00277778h; microwave irradiation;

DOI:10.1039/a900309f

upstream raw materials:

piperonal

Downstream raw materials:

2-Benzo[1,3]dioxol-5-yl-imidazo[1,2-a]pyridin-3-ylamine

2-(benzo[d][1,3]dioxol-6-yl)-2-hydroxyacetonitrile

piperonal

1-(3,4-methylenedioxyphenyl)-2-aminoethanol

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