1-N-BUTYL-2-PHENYLBENZIMIDAZOLE

Base Information

• Chemical Name: 1-N-BUTYL-2-PHENYLBENZIMIDAZOLE
• CAS No.: 24107-62-8
• Molecular Formula: C17H18N2
• Molecular Weight: 250.343
• Mol file: 24107-62-8.mol

Synonyms:1-Butyl-2-phenyl-1H-benzoimidazole;2-phenyl-N-n-butylbenzimidazole;1-N-BUTYL-2-PHENYLBENZIMIDAZOLE;1-butyl-2-phenylbenzimidazole;

Chemical Property of 1-N-BUTYL-2-PHENYLBENZIMIDAZOLE

Chemical Property:

• PSA: 17.82000
• LogP: 4.50340

Purity/Quality:

99% ^*data from raw suppliers

1-N-BUTYL-2-PHENYLBENZIMIDAZOLE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-N-BUTYL-2-PHENYLBENZIMIDAZOLE

There total 5 articles about 1-N-BUTYL-2-PHENYLBENZIMIDAZOLE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

1-bromo-butane (109-65-9) + 2-phenyl-1H-benzoimidazole (716-79-0) → 1-butyl-2-phenyl-1H-benzo[d]imidazole (24107-62-8)

Guidance literature:

With potassium iodide; potassium hydroxide; In dimethyl sulfoxide; at 20 ℃; for 4h; Cooling;

Reference yield: 89.0%

benzylidene dibromide (618-31-5) + o-amino-N-n-butylaminobenzene (51592-02-0) → 1-butyl-2-phenyl-1H-benzo[d]imidazole (24107-62-8)

Guidance literature:

With potassium tert-butylate; iodine; dibenzoyl peroxide; In pyridine; N,N-dimethyl-formamide; for 2h; Reflux;

DOI:10.1016/j.tetlet.2010.09.080

Reference yield: 73.0%

N-benzyl-N′-butylbenzene-1,2-diamine → 1-butyl-2-phenyl-1H-benzo[d]imidazole (24107-62-8)

Guidance literature:

With iron(III) chloride hexahydrate; In N,N-dimethyl-formamide; at 90 ℃; for 4h;

DOI:10.1021/acs.joc.9b02714

upstream raw materials:

1-bromo-butane

2-phenyl-1H-benzoimidazole

benzylidene dibromide

o-amino-N-n-butylaminobenzene

Downstream raw materials:

N-(n-butyl)-2-(2-bromophenyl)-benzimidazole

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