1-Methoxy-4-(Phenylazo)Naphthalene

Base Information

• Chemical Name: 1-Methoxy-4-(Phenylazo)Naphthalene
• CAS No.: 24390-69-0
• Molecular Formula: C17H14N2O
• Molecular Weight: 262.311
• Hs Code.: 2927000090
• European Community (EC) Number: 661-015-1
• DSSTox Substance ID: DTXSID00408143
• Nikkaji Number: J325.199C
• Mol file: 24390-69-0.mol

Synonyms:1-Methoxy-4-(Phenylazo)Naphthalene;24390-69-0;(4-methoxynaphthalen-1-yl)-phenyldiazene;Diazene, (4-methoxy-1-naphthalenyl)phenyl-;SCHEMBL3285471;1-Methoxy-4-phenylazonaphthalene;DTXSID00408143;AKOS024340972;FT-0735675;(4-METHOXYNAPHTHALEN-1-YL)(PHENYL)DIAZENE

Chemical Property of 1-Methoxy-4-(Phenylazo)Naphthalene

Chemical Property:

• Vapor Pressure: 2.21E-07mmHg at 25°C
• Boiling Point: 435.5oC at 760 mmHg
• Flash Point: 174.8oC
• PSA: 33.95000
• Density: 1.11g/cm3
• LogP: 5.26380
• XLogP3: 4.9
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 262.110613074
• Heavy Atom Count: 20
• Complexity: 325

Purity/Quality:

1-METHOXY-4-(PHENYLAZO)NAPHTHALENE Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COC1=CC=C(C2=CC=CC=C21)N=NC3=CC=CC=C3

Technology Process of 1-Methoxy-4-(Phenylazo)Naphthalene

There total 9 articles about 1-Methoxy-4-(Phenylazo)Naphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dimethyl sulfate (77-78-1) → 1-phenylazo-4-methoxynaphthalene (24390-69-0)

Guidance literature:

With sodium hydroxide;

Reference yield:

methyl iodide (74-88-4) → 1-phenylazo-4-methoxynaphthalene (24390-69-0)

Guidance literature:

With ethanol;

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + 4-Phenylazo-1-naphthol (3651-02-3) → 1-phenylazo-4-methoxynaphthalene (24390-69-0)

Guidance literature:

With diethyl ether;

upstream raw materials:

diazomethane

4-Phenylazo-1-naphthol

dimethyl sulfate

methyl iodide

Downstream raw materials:

4-methoxy-1,2-naphthoquinone

4-ethoxynaphthalene-1,2-dione

[1,4]naphthoquinone

benzene

Refernces

• 1、 Yoshida, Katsuhira,Koujiri, Tetsunao,Horii, Taeko,Kubo, Yuji. "Photochromic Properties of Unsymmetric Mono- and Bis(phenylazo)naphthalenes". . p. 1658 - 1664. Retrieved 2007/10/02.