Benzene, 5-bromo-2-methoxy-1-(methoxymethoxy)-3-methyl-

Base Information

Chemical Name:Benzene, 5-bromo-2-methoxy-1-(methoxymethoxy)-3-methyl-
CAS No.:244126-25-8
Molecular Formula:C10H13BrO3
Molecular Weight:261.115
Hs Code.:
DSSTox Substance ID:DTXSID00458426
Nikkaji Number:J1.155.652C
Wikidata:Q82281693
Mol file:244126-25-8.mol

Synonyms:244126-25-8;Benzene, 5-bromo-2-methoxy-1-(methoxymethoxy)-3-methyl-;SCHEMBL13116219;DTXSID00458426;1-(Methoxymethoxy)-2-methoxy-3-methyl-5-bromobenzene

Suppliers and Price of Benzene, 5-bromo-2-methoxy-1-(methoxymethoxy)-3-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 0 raw suppliers

Chemical Property of Benzene, 5-bromo-2-methoxy-1-(methoxymethoxy)-3-methyl-

Chemical Property:

PSA：27.69000
LogP:2.74880
XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:4
Exact Mass:260.00481
Heavy Atom Count:14
Complexity:165

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=CC(=C1OC)OCOC)Br

Technology Process of Benzene, 5-bromo-2-methoxy-1-(methoxymethoxy)-3-methyl-

There total 5 articles about Benzene, 5-bromo-2-methoxy-1-(methoxymethoxy)-3-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 107-30-2
chloromethyl methyl ether

: 244229-56-9
5-bromo-2-methoxy-3-methyl-phenol

: 244126-25-8
5-bromo-2-methoxy-1-methoxymethoxy-3-methyl-benzene

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃;
DOI:10.1055/s-1999-3161

Reference yield:

: 488-17-5
3-methylbenzene-1,2-diol

: 244126-25-8
5-bromo-2-methoxy-1-methoxymethoxy-3-methyl-benzene

Guidance literature:: Multi-step reaction with 5 steps

1: 83 percent / TEA / CH₂Cl₂ / 0 °C

2: 97 percent / Br₂; AcOH / CH₂Cl₂ / 0.5 h / 20 °C

3: 96 percent / K₂CO₃ / acetone / 1 h / Heating

4: 97 percent / aq. NaOH / ethanol / 0.5 h / Heating

5: 97 percent / i-Pr₂NEt / CH₂Cl₂ / 0 - 20 °C

With sodium hydroxide; TEA; bromine; potassium carbonate; acetic acid; N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane; acetone;
DOI:10.1021/ja026216d

Reference yield:

: 244126-23-6
toluene-4-sulfonic acid 5-bromo-2-hydroxy-3-methyl-phenyl ester

: 244126-25-8
5-bromo-2-methoxy-1-methoxymethoxy-3-methyl-benzene

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / K₂CO₃ / acetone / 1 h / Heating

2: 97 percent / aq. NaOH / ethanol / 0.5 h / Heating

3: 97 percent / i-Pr₂NEt / CH₂Cl₂ / 0 - 20 °C

With sodium hydroxide; potassium carbonate; N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane; acetone;
DOI:10.1021/ja026216d