N-Ethylhypochlorous amide

Base Information

• Chemical Name: N-Ethylhypochlorous amide
• CAS No.: 24948-82-1
• Molecular Formula: C2H6ClN
• Molecular Weight: 79.5293
• Hs Code.: 2921199090
• DSSTox Substance ID: DTXSID90510562
• Nikkaji Number: J25.735D
• Wikidata: Q82368906
• Mol file: 24948-82-1.mol

Synonyms:N-Ethylhypochlorous amide;chloro-ethylamine;24948-82-1;ethylamino hydrochloride;DTXSID90510562;ZPQILRVCDUDSEB-UHFFFAOYSA-N

Chemical Property of N-Ethylhypochlorous amide

Chemical Property:

• Boiling Point: 47.8±23.0 °C(Predicted)
• PKA: 0.30±0.70(Predicted)
• PSA: 12.03000
• Density: 0.972±0.06 g/cm3(Predicted)
• LogP: 1.14060
• XLogP3: 0.5
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 79.0188769
• Heavy Atom Count: 4
• Complexity: 10

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCNCl

Technology Process of N-Ethylhypochlorous amide

There total 9 articles about N-Ethylhypochlorous amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

ethylamine (75-04-7,85404-22-4) → N,N-dichloroethylamine (24948-83-2) + N-chloroethylamine (24948-82-1)

Guidance literature:

With N-chloro-succinimide; Adipic acid; at 20 ℃; under 0.1 Torr; Title compound not separated from byproducts;

DOI:10.1055/s-1985-31450

Reference yield: 80.0%

ethylamine (75-04-7,85404-22-4) → N-chloroethylamine (24948-82-1)

Guidance literature:

With sodium hypochlorite; sodium hydrogencarbonate; In water; at 0 - 5 ℃;

DOI:10.1007/s11172-006-0291-2

Reference yield: 67.5%

5-Methyl-2-(2-methyl-propane-2-sulfonyl)-benzene-1,3-dicarbaldehyde dioxime (126076-87-7) → N-chloroethylamine (24948-82-1)

Guidance literature:

With tert-butylhypochlorite; In water; tert-butyl alcohol; at -10 ℃; for 1.5h;

DOI:10.1007/BF00957792

upstream raw materials:

ethanamine hydrochloride

ethylamine

N-ethyl-1,1,1-trimethylsilanamine

5-Methyl-2-(2-methyl-propane-2-sulfonyl)-benzene-1,3-dicarbaldehyde dioxime

Downstream raw materials:

acetaldehyde

N,N-dichloroethylamine

ethylamine

1,2-diethyldiaziridine